... methylenedioxide ( H 5,89, d (1 ,4); 5,86, d (1 ,4); δC 100,50, C-19) có nhánh angeloyl ho c tigloyl ñư c th y rõ qua c m tín hi u δC 165,78 (C-1’); 127,06 (C-2’); 139,87 (C-3’); 15,64 (C-4’); 19,69 (C-5’) ... ng là: n-hexan SSH (7 3,8 gam), chloroform SSC (4 9,7 gam), ethyl acetat SSE (5 ,5 gam) nbutanol SSB (3 ,1 gam) (Sơ ñ 2.1) 2.3.1.1 C n chi t n-hexan SSH C n chi t n-hexan SSH (7 3,8 gam) ñư c kh o ... n-hexan/ethyl acetat (t l : 9/1 → 1/9), thu ñư c 16 phân ño n (ký hi u là: SSH01 → SSH16) (Sơ ñ 2.2) Qu Ngũ v t Thu, x lí C n chi t SSH B t qu khô (1 ,85 kg) (7 3,8 g) 1.Chi t b ng methanol (3 l n) 2.C...