Drugs and Poisons in Humans - A Handbook of Practical Analysis (Part 21)
Drugs and Poisons in Humans - A Handbook of Practical Analysis (Part 21)
... 3.4206 Morphine and its analogues 8) Matsubara K, Fukushima S, Akane A et al. (1992) Increased urinary morphine, codeine and tetrahydropapavero-line in Parkinsonian patient undergoing L-3,4-dihydroxyphenylalanine ... conjugated forms of opiates, the authentic standards of mor-phine-3-glucuronide (M-3-G) and morphine-6-glucuronide (M-6-G) are necessary. In U.S .A. and Europe, it is easy to obtain these authentic ... Nakajima K, Igarashi K et al. (1992) Analysis of morphine-3-glucuronide in urine by LC/APCI-MS. Eisei Kagaku 38:121–126 (in Japanese with an English abstract) 14) Tatsuno M, Nishikawa M, Katagi...
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Drugs and Poisons in Humans - A Handbook of Practical Analysis (Part 17)
... mg/mL), and kept airtightly in a refrigerator. A 5- L volume of the above solution is placed using a microsyringe in a glass vial containing 1 mL of dimethyl sulfoxide (DMSO), capped airtightly and ... transformation in rats. J Pharm Sci 74:780–782 10) Kielbasa WB, Bauer JA, Fung HL (1999) Analysis of isobutyl nitrite inhalant in rat and human blood: application for pharmacokinetic investigations. ... manufacturing drugs or as reagents for synthesis in industries; they are also used as aromatics. Because of their pharmacological e ect, alkyl nitrites are being abused as uncontrolled inhalant drugs...
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Drugs and Poisons in Humans - A Handbook of Practical Analysis (Part 67)
... done inside a dra chamber.f) For quantitative analysis of DAEMS, various concentrations of DAEMS are spiked into blank serum specimens containing a xed amount of DAEMO (IS) each and extracted ... DAEMS consisting of peak area ratio of DAEMS to IS on the vertical axis and DAEMS concentration on the horizontal axis. A peak area ratio obtained from a test specimen is applied to the calibration ... be evaporated at a lower temperature gradually and carefully. If VX itself remains, there is a danger of the secondary exposure for an analyst; the manipulations including the above evaporation...
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Drugs and Poisons in Humans - A Handbook of Practical Analysis (Part 20)
... GC/MS analysis of ∆9-THC-11-oic acid in urine 188 Cannabinoids and their metabolites GC analysis of cannabinoids in plant specimens a Reagents and their preparation• Extraction and puri cation ... disposition, and kinetics of delta-9-tetrahydrocannabinol in men and women. Clin Pharmacol Ther 34:352–363 2) Agurell S, Halldin M, Lindgren J-E et al. (1986) Pharmacokinetics and metabolism of ∆1-tetrahydrocannabinol ... metabolites. Acta Pharm Suec 16:21–33 9) Yamamoto I, Watanabe K, Narimatsu S et al. (1990) A GC-MS method for determination of ∆9-tetrahydrocanna-binol-11-oic acid in human urine. Eisei Kagaku...
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Drugs and Poisons in Humans - A Handbook of Practical Analysis (Part 70)
... methemoglobinemia be-comes severe, it causes cyanosis, headache, easy fatigability, respiratory and conciousness dis-turbances and nally death. e fatal methemoglobinemia is rare, but fatal ones a ... (1987) Cyanosis in infants caused by nitrates in well water. JAMA 257:2788–2792 12) Fan AM, Steinberg VE (1996) Health implications of nitrate and nitrite in drinking water: an update on methe-moglobinemia ... was disclosed that he had ingested nitrate. e analytical results for nitrite and nitrate in his blood and stomach contents are shown in > Table 5.2. An example of the gas chromatograms...
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Drugs and Poisons in Humans - A Handbook of Practical Analysis (Part 71 and End)
... 3851-amino- 4- phenylbutane 1732-amino-6-hydroxymethyl-8-hydroxyquinazoline 482aminomethyl phosphonic acid 5467-aminonitrazepam 195-aminoquinoline 499amitriptyline 271, 274, 276amniotic ... 327N-de-ethyl-LSD 228n-decane 165n-heptane 165n-hexane 165N-methyl- 1-( 3,4-methylene-dioxyphenyl )-2 -butan-amine 229N-methyl- 1-( 3,4-methylene-dioxyphenyl )-3 -butan-amine 233N-methyl-bis(tri uoro-acetamide) ... 285, 290alternative specimens 9Amanita neoovoidea 480Amanita pantherina 469Amanita phalloides 469Amanita verna 469, 474Amanita virosa 469, 473amanitin 473, 477, 479amido-type local anesthetic...
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Drugs and Poisons in Humans - A Handbook of Practical Analysis (Part 22)
... mass spectra of the authentic cocaine, EME and BE a er derivatization.Setting up of cuto values are very common in USA and Europe as a part of QC ( quality control) and QA ( quality assurance) ... of BE in blood, a satisfactory mass spectrum can be obtained. For BE, Metabolic pathways of cocaine.⊡ Figure 4.4Toxic and fatal concentrations212 Cocaine and its metabolites and tablets of ... on average for urine sampled 0–1 h a er cocaine inhalation; the ratio was 10.6 on average for urine sampled 0–8 h a er the inhalation. e ratios increased according to the increase in time...
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Drugs and Poisons in Humans - A Handbook of Practical Analysis (Part 23)
... concentration in the horizontal axis and peak area ratio of pentazocine to IS in the vertical axis. e peak area ratio of a test specimen is applied to the calibration curve to obtain its pentazocine ... Dextromethorphan-HBr to be used as internal standard (IS) was purchased from Sigma; Sep-Pak C18 cartridges (classic type) from Waters 222 PentazocineSIM chromatograms for pentazocine (peak 2) and ... cases of pentazocine abuse especially for medical and co-medical workers. e drug is being regulated as a subclass compound of narcotics (DEA class: IV).Pentazocine in both antemortem and postmortem...
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Drugs and Poisons in Humans - A Handbook of Practical Analysis (Part 24)
... digestive tract is rapid and distinct visual hallucination takes place 45 min–1 h a er oral intake of about 20 µg of LSD [1]. e hallucination becomes most marked 2–3 h a er the intake and lasts ... powerful hallucinogenic drugs of abuse. LSD was explosively abused in U.S .A. in the latter half of the 1960s. In Japan, the amount of seizure of LSD is much smaller than that of methamphetamine. ... under an o cial transfer process. • p-Dimethylbenzaldehyde reagent: a 0.125-g aliquot of p-dimethylaminobenzaldehyde (Wako Pure Chemical Industries, Ltd., Osaka, Japan and other manufacturers)...
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Drugs and Poisons in Humans - A Handbook of Practical Analysis (Part 25)
... MDAs and their main metabolites 4-hydroxy-3-me-thoxymethamphetamine ( HMMA) and 4-hydroxy-3-methoxyamphetamine ( HMA) in urine specimens are presented.Metabolic pathways for MDMA and MDA.⊡ ... H, Nakajima K, Nishikawa M et al. (1991) Determination of methamphetamine and amphetamine in urine by headspace gas chromatography/mass spectrometry. Anal Sci 7:19–22 25) Shima N, Kamata T, ... per tablet) as the primary ingredient, sometimes smaller amounts of amphetamines and/ or other pharmaceutical agents, such as ca eine and ketamine [4, 5].Structures of MDA and its analogues.⊡...
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