mcreynolds constants for stationary phases in gas chromatography
Synthesis of crown ether and cyclam capped beta cyclodextrin bonded silica particles and their application as chiral stationary phases in liquid chromatography
... One drawback in utilizing cyclodextrins is the low binding constants for most guest molecules [94] It was reported that diaza-18-crown-6 capped β-CD exhibited high binding constants for several ... molecular cavities in which solute molecules can enter and interact with neighboring groups (5) Cyclodextrin-based chiral stationary phases These stationary phases contain cyclodextrin-based materials ... Chiral Stationary Phases for Liquid Chromatography 1.3.1 Types of Chiral Stationary Phases for Liquid Chromatography 1.3.2 Preparation of β-Cyclodextrin Type of Chiral Stationary Phases 10 ii 1.4...
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ENANTIOSEPARATION OF CHIRAL DRUGS IN LIQUID CHROMATOGRAPHY WITH ANTIBIOTIC CAPPED MACROCYCLE BONDED SILICA PARTICLES AS CHIRAL STATIONARY PHASES
... own the wisdom of thinking Beyond the overwhelming experience of reading journals, staying up for experiments, giving presentations and writing papers, it is truly a training process to learn ... selectivity in chromatography In addition, β-CD was reported to use as CMPA for vancomycin-based CSP in LC achieved better enantioseparation performance for duloxetine than vancomycin-based CSP ... building blocks The nomenclature of calixarene is straightforward to count the number of repeating units in the ring and include it in the name, i.e calix[4]arene has four units in the ring The...
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Determination of EDTA in Water Samples by SPE-Gas Chromatography/Mass Spectrometry
... water was used in all experiments Gas chromatography/ mass spectrometry analysis Gas chromatography was carried out by using HP6890 series gas chromatography system (Hewlett Packard, Wilmington, DE, ... acid (EDTA) in Drinking-water, Background document for development of WHO Guideline for Drinking-water Quality, 2nd ed Addendum to vol Health criteria and other supporting information, World Health ... was 70ºC as initial temperature for min; ramped at 15ºC/min to 300ºC then held at 300ºC for The carrier gas (helium) flow rate was set at 1.2 mL/min Mass spectrometry was carried out using a 5973...
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DETERMINATION OF ORGANIC COMPOUNDS IN DRINKING WATER BY LIQUID-SOLID EXTRACTION AND CAPILLARY COLUMN GAS CHROMATOGRAPHY/MASS SPECTROMETRY pdf
... hydrocarbons (PAH), including the labeled PAHs used in this method as internal standards, are rapidly oxidized and/or chlorinated in water containing residual chlorine Therefore, residual chlorine must ... container with water from a representative area Sampling equipment, including automatic samplers, must be free of plastic tubing, gaskets, and other parts that may leach interfering analytes into ... the sample into the solvent reservoir The water sample will drain into the cartridge, and from the exit into the suction flask Maintain the packing material in the cartridge immersed in water at...
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CHEMICAL REACTIONS IN GAS, LIQUID AND SOLID PHASES: SYNTHESIS, PROPERTIES AND APPLICATION pptx
... hydrolysis by celloviridin complex Phenosan in the form of industrially produced acid is used in cattle breeding by inducing the growth-stimulating action in the forage composition for the farm livestock ... described in Ref 15 The interval from the beginning of the experience to the point of intersection of two straight lines for which tg α1 = tg α2 was taken as τ in the presence of InH The first line ... damages in connection with or arising out of information contained in this book The Publisher shall not be liable for any special, consequential, or exemplary damages resulting, in whole or in part,...
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ADVANCED GAS CHROMATOGRAPHY – PROGRESS IN AGRICULTURAL, BIOMEDICAL AND INDUSTRIAL pdf
... Diethyleneglycol succinate (DEGS) 496 746 590 837 835 Table McReynolds constants values for some usual stationary phases Currently there are hundreds of stationary phases used in gas chromatography and McReynolds ... with olefins Chiral stationary phases, containing chiral compounds interacting with only one optical isomer of a pair of enantiomers Such phases are based on cyclodextrin or certain amino acids ... (C); Liquid chromatography (LC); Gas chromatography (GC); Paper chromatography (PC); Thin-layer chromatography (TLC) Column chromatography (CC) Gas- liquid chromatography (GLC); Gas- solid chromatography...
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ASTM D2887 Standard Test Method for Boiling Range Distribution of Petroleum Fractions by Gas Chromatography
... hundred parts of CS2 TABLE Boiling Points of Normal ParaffinsA,B Carbon Number Boiling Point, °C Boiling Point, °F Carbon Number Boiling Point, °C Boiling Point, °F 10 11 12 13 14 15 16 17 18 19 ... recording the time of each peak maximum and the boiling point temperature in degrees Celsius (or Fahrenheit) for every component in the mixture n-Paraffin boiling point temperatures are listed in ... temperature (°C) Final column temperature (°C) Oven programming rate (°C/ min) Detector Detector temperature (°C) Injector Injector initial temperature (°C) Injector programming rate (°C/ min) Injector...
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Marketing strategy of petrolimex gas JSC for bottled liquefied petrolium gas in Ho Chi Minh city 2012 to 2015
... cheaper in some applications In Vietnam, LPG in cylinder or bottled LPG is used almost in resident domain and LPG in tank is used in industrial fields There are three kinds of LPG product in bottle: ... installed City Gas pipeline system cover all cities Vietnam in general and HCMC in particular, mostly use bottled LPG for cooking, heating…According research of Rinnai – Burner manufacturer in ... system of LPG trading companies, serving LPG supply to the Ho Chi Minh City and surrounding 38 Dang Tran Hanh Thong Final Project provinces The gas cylinder inspection and painting plant with new...
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Development of novel chiral stationary phases for HPLC based on covalently bonded polysaccharide derivatives
... mobile phases containing chloroform, dichloromethane or tetrahydrofuran Optimization of selected racemic analytes is realized on various CSPs in chloroform-containing, dichloromethane-containing, ... on CSP AzCPC-1.5I2 in CHCl3-containing mobile phases and CH2Cl2-containing mobile phases 92 Figure 3.14 Chromatograms of 4, 5c, and 13 on CSP AzCPC-1.5I2 in CH2Cl2-containing mobile phase series ... a combination of two forces: i) hydrogen bondings, π-π interactions and dipole interactions, which are typical in type I CSPs; and ii) formation of inclusion complex into cavities or ravines,...
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Design and analysis of object allocation and replication algorithms in distributed databases for stationary and mobile computing systems
... request */ {Service the requests in win(o); /*win(o) is empty after servicing*/ Insert Req into win(o); T Co = τ ; } } } For (Each currently existed request window win(o ) in the system) /* No matter ... future phases It may be noted that DWM algorithm need not wait for the entire window win(o) to be filled up for processing Following example will clarify the working policy of the window mechanism in ... all the processors in S(o), incurring (|S(o)|)Cd units of cost Finally, in both the cases, servers in S(o) will save the object o into their respective local memories, incurring a total of |S(o)|...
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Determination of endocrine disrupting compounds in environmental samples using microextraction combined with gas chromatography mass spectrometry
... follows: initial temperature 50ºC, held for min, then increased by 20ºC min-1 to 100ºC, a second increase at 10ºC min-1 to 200ºC, and a third increase at 20ºC min-1 to 300ºC held for minutes The ... known major contributing factors to the burden of PAH in the environment [23, 24] For example, during the widespread forest fire incident in Indonesia in 1997, air quality in Southeast Asia was ... headspace of a solution containing 200 µl of BSTFA in ml of acetone (in a 10-ml vial) for 10 minutes at 70ºC The fiber was then desorbed in the injection port of the GC for minutes Figure 2.1.1 shows...
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Novel chiral stationary phases (CSP) for enantioseparation processes
... and an isoelectric point of 4.8 Two major drug-binding sites, the warfarin-azapropazone site and the benzodiazapine-indole binding site are believed to exist in the protein The column has proved ... Cyclodextrin-based chiral stationary phases (CD-CSPs) In 1965, Solms and Egli107 reported the first preparation of insoluble CD polymers-epichlorohydrin resins and their selectivity in binding various ... In the research area, analytical methods capable of discriminating enantiomers are employed in many fields Some examples are investigating products, monitoring asymmetric synthesis, determining...
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Big spenders the outlook for the oil and gas industry in 2012
... outlook for the oil and gas industry in 202 Big spenders The outlook for the oil and gas industry in 2012 66 Refining Better daysRefining ahead? Better days ahead? Key points Key points l Refining ... provision breaks, a s worldwide, worldwide, including worldwide, interests including including in interests China, interests eastern in in China, China, eastern eastern concern that the depletion ... outlook oil outlook and for gas for the industry the oiloil and and ingas 202 gas industry industry inin 202 202 Big spenders The outlook for the oil and gas industry in 2012 Big spenders Figure...
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Deep water ahead the outlook for the oil and gas industry in 2011
... recovery of gas demand “The excess of gas that pushed gas market prices downwards in 2009 should continue to decline in 2011, owing to the recovery of gas demand growth in Asia and in the emerging markets ... companies invested heavily in US shale gas, including through large acquisitions, throughout 2009 This investment has continued into 2010, despite declining prices For example, Statoil (Norway), in ... roughly in line with the Economist Intelligence Unit’s forecasts This uncertainty about price hinges on a range of factors One is the changing demand situation in Asia, and in particular China Gas...
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Báo cáo y học: "Characterization of Human Erythrocytes as Potential Carrier for Pravastatin: An In Vitro Study"
... the loading of pravastatin into erythrocytes was directly proportional with increase of drug concentration in the incubation medium, in the 2-10 mg/ml concentration range This finding is in concurrence ... statins including inhibition of the metabolism [5], administration of statins with certain juices [6] or inhibition of Pgp [3] Unfortunately these strategies are frequently associated with increase ... Pharmacokinetic-pharmacodynamic drug interactions with HMG-CoA reductase inhibitors Clin Pharmacokinet 2002; 41(5):343-370 Hatanaka T Clinical pharmacokinetics of pravastatin: mechanisms of pharmacokinetic...
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Báo cáo y học: "Comparison between single antiplatelet therapy and combination of antiplatelet and anticoagulation therapy for secondary prevention in ischemic stroke patients with antiphospholipid syndrome"
... high-intensity warfarin (INR over 3.0) with or without low-dose aspirin (75 mg/day) was significantly more effective than low-intensity warfarin (INR under 3.0) with or without low-dose aspirin, ... serum obtained from patients with positive IgG cardiolipin antibodies interfered with protein C activation [2] Protein C activation is disturbed in patients with APS [17] Since protein C is closely ... cerebral hemorrhage was noted in the single antiplatelet therapy group, and one subcutaneous hemorrhage was found in the combination therapy group As for the patient in the single antiplatelet therapy...
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Báo cáo y học: "Efficiency of vibration exercise for glycemic control in type 2 diabetes patients."
... against the swinging platform.The number of sets was identical with the strength training regimen It took about 20 minutes to fulfill a training session of the last three weeks Table 1: Baseline ... pre-training, hollow bars = post-training mean ± SE Figure 4: Glucose plasma-concentrations during OGTT before (black) and after the training period (hollow) Left top: Flexibility training group, ... After training intervention, fasting glucose concentrations were slightly reduced in all groups (n.s., Tab 2) Within the 150 minutes observation period of OGTT, pre- and posttraining results in the...
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Towards a combined product - process approach TO DEVELOPING BUSINESS CORRESPONDENCE WRITING SKILLS FOR ENGLISH MAJORS IN HAIPHONG UNIVERSITY
... note that with the increasing numbers of international students taking Master courses in Business, Finance, Accounting and Banking, the area of Academic Business English is beginning to assume much ... but correct business letters, memos, faxes and reports - To participate in business contexts giving personal information, exchanging information and expressing opinions 2.1.2 The business English ... learning English as most respondents (38/42) accounting for 90% say that they study English for finding a good job in the future The remaining accounting for 10% claim that they study English for...
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