... the time of collection untilextraction. Fill the sample bottles and, if residual chlorine is present, add 80 mg of sodium thiosulfate per liter of sample and mix well. EPA Methods 330.4 and 330.5 ... “Microdetermination of Derivatives of Phenols and Mercaptans byMeans of Electron Capture Gas Chromatography,” Analytical Chemistry, 40, 1009 (1968).4. ASTM Annual Book of Standards, Part 31, D3694-78. “Standard ... stock standards to avolumetric flask. To each calibration standard, add a known constant amount of one or more internal standards, and dilute to volume with 2-propanol. One of the standards...