Chita : A Memory of Last Island This Etext ppt

... wild cane, and marsh grasses. For, at a hasty glance, the general appearance of this marsh verdure is vague enough, as it ranges away towards thesand, to convey the idea of amphibious vegetation, ... tells of hereditary refinement of habit and of mind: a natural grace, a thorough-bred ease and elegance of movement, a quickness and delicacy of perception.She became strong again and active active ... Orleans, a veteran steamboat man and a market contractor, to whom he had disposed of many a cargo of fresh pompano,sheep's-head, and Spanish-mackerel Harris was the first to step to land;...

Tài liệu Drugs and Poisons in Humans - A Handbook of Practical Analysis (Part 27) ppt

... concentration on the horizontal axis and of peak area ratio of a drug to IS on the vertical axis.  e above peak area ratio obtained from a specimen is applied to the calibration curve to obtain ... MO, USA). Pure powder of perazine and clospi-razine was donated by Mitsubishi Welpharma, Osaka, Japan; that of  upentixol by Takeda Chem. Ind. Ltd., Osaka, Japan; that of thioproperazine by ... chromatograph (Agilent Technologies, Palo Alto, CA, USA); mobile phase A: distilled water containing 0.1 % formic acid and 10 mM 259ammonium acetate; mobile phase B: 100 % acetonitrile. A gradient...

Tài liệu Drugs and Poisons in Humans - A Handbook of Practical Analysis (Part 28) pptx

... ButyrophenonesHPLC analysisInstrument: an SPD-M1 0A photodiode array detector ( DAD), a CTO-1 0A column oven, an SIL-1 0A autosampler and an LC-10AD pump system (all from Shimadzu Corp., Kyoto, Japan).HPLC ... spiked to blank blood or urine to draw a calibration curve. A peak area ratio of a test specimen is applied to the calibration curve to calculate its concentration.Assessment of the method ... detection and quantitation of haloperidol and seven of its metabolites in microsomal preparations. J Chromatogr B 61 4:2 67–273 12) Aravagiri M, Marder SR, Van Putten T et al. (1994) Simultaneous...

Tài liệu Drugs and Poisons in Humans - A Handbook of Practical Analysis (Part 29) ppt

... antidepressants and carbamazepine obtained by HPLC-UV. A: carbamazepine, B: desipramine, C: maprotiline, D: nortriptyline, E: amoxapine, F: setiptiline, G: mianserin, H: imipramine, I: amitriptyline, ... Japanese) 3) Tanaka E, Terada M, Nakamura T et al. (1997) Forensic analysis of eleven cyclic antidepressants in human biolo-gical samples using a new reversed-phase chromatographic column of ... Kimura T (1999) A fatal case of carbamazepine poisoning. Jpn J Toxicol 1 2:6 5–68 (in Japanese with an English abstract) 7) Pfleger K, Maurer HH, Weber A (1992) Mass Spectral and GC Data of Drugs,...

Tài liệu Drugs and Poisons in Humans - A Handbook of Practical Analysis (Part 31) ppt

... Tanaka E, Nakamura T, Nagashima A et al. (2001) Determination of plasma bromvalerylurea and its main meta-bolite by a simple high-performance liquid chromatographic method and quantitation of ... bromide and urea: 5 g of 2-bromohexanoyl bromide (Aldrich, Milwaukee, WI, USA) and an equimolar amount of urea are placed in a 100 mL volume eggplant-shaped glass  ask and warmed in a water bath ... screening of drugs in biological materials by gas chromatography and gas chromatography-mass spectrometry. A fatal poisoning by ingestion of a drug containing acetaminophen, ethenzamide and bromvaleryurea....

Tài liệu Drugs and Poisons in Humans - A Handbook of Practical Analysis (Part 32) ppt

... µg/mL. 1: barbital; 2: allobarbital; 3: metharbital; 4: phenobarbital; 5: cyclobarbital; 6: pentobarbital; 7: hexobarbital; 8: amobarbital; 9: secobarbital; 1 0: thiopental; 1 1: IS [ 5-(4-methylphenyl)-5-phenylhydantoin].⊡ ... activated charcoal. JAMA 24 7:2 400–2401 24) Furuno J, Sugawara N (1972) On a fatal case of thiopental shock and the metabolism. Jpn J Legal Med 2 6:7 1–77 (in Japanese with an English abstract) ... Upon arrival at a hospital, blood phenobarbital concentration was as high as 107 µg/mL. As emergency treatments, 30 g of activated charcoal and 30 g of sodium sulfate were administered orally....

Tài liệu Drugs and Poisons in Humans - A Handbook of Practical Analysis (Part 37) pptx

... diazepam.353 HPLC analysis of antiepileptics and some metabolites in plasma [15]Reagents and their preparation• Ethosuximide, primidone, phenobarbital, carbamazepine, phenytoin and carbamazepine-epoxide ... kinds of antiepileptics ( ethosuximide, primidone, lamotrigine, phenobarbi-tal, phenytoin and carbamazepine) and two carbamazepine metabolites ( carbamazepine-diol and carbamazepine- epoxide) can ... reference [6].d) Lamotrigine and carbamazepine-diol are not obtainable in Japan; the analytical data of these compounds has been shown only as useful informations.e) For extraction of antiepileptics...

Tài liệu Drugs and Poisons in Humans - A Handbook of Practical Analysis (Part 38) pptx

... ➁ : methanol/tetrahydrofuran/5 % formic acid ( 7:7 :6 , v/v); ➂ : methanol/chloroform/acetic acid ( 5:4 :1 , v/v); ➃ : Dragendorff reagent; ➄ : iodoplatinate reagentTLC analysis362 Muscle relaxants ... ammonium acetate/acetoni-trile can be used. With ODS-type columns, tri uoroacetic acid can be added to a mobile phase as an ion-pairing reagent for analysis of the quaternary amino muscle relaxants ... solid-phase extraction of the drugs, weak cation-exchanger cartridges are used. In this case, the packing material is of carboxylic acid-type. When strong cation-exchanger cartridges of sulfonic acid-type...

Tài liệu Drugs and Poisons in Humans - A Handbook of Practical Analysis (Part 39) ppt

... uoroacetic anhydride, a base peak at a higher mass number due to a TFA derivative of a β-blocker can be obtained a er heating and evaporation of the excess reagent; for example, the mass spectrum ... concentrations of the authentic standard of a drug and the IS, and are processed according to the above procedure to construct each calibra-tion curve. By applying the peak area ratio of a specimen ... β-receptors; they cause hypotension by decreasing the heart beat rate and cardiac output, and prevent the attacks of arrhythmia and angina pectoris. In the brain, the drugs attenuate migraine by suppressing...

Tài liệu Drugs and Poisons in Humans - A Handbook of Practical Analysis (Part 43) pptx

... solutions are analyzed by the above CE to construct a calibration curve (concentration of a hypochlorite ion in a specimen vs. peak area). A peak area obtained from a specimen is applied to the calibration ... conditions: an HP3DCE system (Yokogawa Analytical Systems, Tokyo, Japan); bu er solution: HP Basic Anion Bu er; column temperature: 30 °C; impressed voltage: –30 kV; detection: indirect absorption ... cases, due to accidental ingestion of hypochlorite and due to inhalation of chlorine gas produced upon mixing a hypochlorite salt with an acidic solution, are relatively many.  e toxicity of...

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