... 40).Figure 23. Superimposed XRPD of anhydrous Forms II, I, V, VI, III, and IV (samples 46, 33, 62, 40, 49, and 57, respectively,bottom to top).Vol. 11, No. 5, 2007 / Organic Process Research & ... Salt to Form VI by Reflux in Acetone. Into a 1-L, three-necked,round-bottomed flask, fitted with an overhead stirrer and a refluxcondenser, were put 1 disodium salt (25.00 g, as mixture ofForm I and ... Behavior of an Organic CompoundUsing a Dynamic Thermal and X-ray Powder Diffraction TechniqueDavid Albers, Michelle Galgoci, Dan King, Daniel Miller,Robert Newman, Linda Peerey, Eva Tai, and Richard...