virtual work method of beam analysis
Báo cáo y học: "Evaluation of Fractional Analysis of Bronchoalveolar Lavage Combined with Cellular Morphological Features"
Ngày tải lên :
03/11/2012, 11:48
...
of disease in sarcoidosis or HP. In addition, finding of
encapsulated exudates may suggest desquamation of
early stage of Masson body which implies possible
diagnosis in a limited number of ... infiltration of mast cells
implies histological feature of organization of colla-
genous matrices or interstitial fibrosis
10
. Basophilic
leukocytes were never found in the normal control
and most of ... interstitial lung
disease.
Conflict of Interest
The authors have declared that no conflict of in-
terest exists.
References
1. Reynolds HY, Newball HH. Analysis of proteins and respira-
tory cells...
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Drugs and Poisons in Humans - A Handbook of Practical Analysis (Part 17)
Ngày tải lên :
18/10/2013, 00:15
... treatment of angina pectoris many years ago
[2]; the pharmacological e ect of the dilation of the coronary arteries was found due to the
action of nitrogen monoxide produced by decomposition of alkyl ... ingestion of 10–15 mL of each alkyl nitrite causes serious methe-
moglobinemia [6]. e LD
50
value for an alkyl nitrite is reported to be 205 mg/kg. ere are not
many cases of analysis of alkyl ... eld of forensic toxicology. In this chapter, the
methods for analysis of the compounds by headspace (HS)-gas chromatography (GC) and
liquid-liquid extraction-GC are presented.
Determination of...
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Drugs and Poisons in Humans - A Handbook of Practical Analysis (Part 67)
Ngày tải lên :
18/10/2013, 00:15
... Paasivirta J et al. (1981) Trace Analysis of Chemical Warfare Agents. An Approach to the
Environmental Monitoring of Nerve Agents. Ministry of Foreign Affairs of Finland, Helsinki, pp 27, 28, ... metabolites of VX, could
be detected [18].
GC/MS analysis for EMPA in serum. (a) a TIC and mass chromatograms; (b) an EI mass spectrum of
the t-BDMS derivative of EMPA; (c) a CI mass spectrum of the ... stream of nitrogen gas at room temperature
e
.
iii. e residue is dissolved in 100 àL of the dichloromethane solution of DAEMO (IS solu-
tion); a 1-àL of it is injected into GC/MS for analysis...
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Drugs and Poisons in Humans - A Handbook of Practical Analysis (Part 20)
Ngày tải lên :
24/10/2013, 19:15
... 10:316–323
14) Yamamoto I (1992) Methods for analysis of cannabis and its components. In: The Pharmaceutical Society of
Japan (ed) Standard Methods of Chemical Analysis in Poisoning – With Commentaries, ... GC/MS analysis of ∆
9
-THC-11-oic acid in human urine
[15, 16].
e) A method of silylation of glassware to be done before analysis was reported [17]; such treat-
ment suppresses the adsorption of ... (1984) Analysis of the major metabolite of ∆
9
-tetrahydrocannabinol in
urine. VI. A comparison of five methods. J Anal Toxicol 8:249–251
12) Baker TS, Harry JV, Russell JW et al. (1984) Rapid method...
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Drugs and Poisons in Humans - A Handbook of Practical Analysis (Part 21)
Ngày tải lên :
24/10/2013, 19:15
... method
Qualitative analysis is made by the comparison of the retention time of a peak of a specimen
with that of the authentic standard and also by the con rmation of the absence of such a peak ... main tool for analysis of opiates
and their metabolites. However, at the present time, GC/MS is being widely used for opiate
analysis.
For HPLC analysis of the conjugated forms of opiates, the ... low levels of morphine starting from a large
amount of a specimen cannot be a proof of the intake of the drug. e level of morphine
in urine of healthy subjects determined by GC/MS was reported...
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Drugs and Poisons in Humans - A Handbook of Practical Analysis (Part 70)
Ngày tải lên :
24/10/2013, 19:15
... action of methemo-
globin reductase (identical with cytochrome b
5
reductase requiring NADH as a cofactor) pres-
ent in mammalian red cells. e concentration of methemoglobin in blood of normal ... is rare, but fatal ones a er ingestion
of nitrate or nitrite were reported [2–6].
For analysis of nitrate or nitrite in blood plasma or serum, the methods by ion chlomatog-
raphy [7] and GC/MS ... derivatization reaction for nitrate being used in this method; 2-nitro-
mesitylene formed is analyzed by GC. e same reaction method is used for analysis of
nitrite a er its conversion into nitrate....
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Drugs and Poisons in Humans - A Handbook of Practical Analysis (Part 71 and End)
Ngày tải lên :
24/10/2013, 19:15
... developed a modi cation of the methods, which enabled accurate determination
of blood Met-Hb even in the presence of high concentrations of CO-Hb by using about a
100-fold excess of potassium ferricynade ... devised a photoelectric method for
determination of Met-Hb in blood. Minor modi cations of this method were made by several
researchers to increase sensitivity [2–4]. ese methods are based on ... determination of carboxyhemoglobin and methemoglo-
bin in victims of carbon monoxide poisoning. J Forensic Sci 25:546–549
6) Sato K, Katsumata Y, Aoki M et al. (1981) A practical method for the...
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Drugs and Poisons in Humans - A Handbook of Practical Analysis (Part 22)
Ngày tải lên :
29/10/2013, 01:15
... aliquot of it is subjected to GC/MS analysis.
Cocaine and its metabolites
215
time of death nor those at the time of samplings. erefore, there are great variation in the fatal
levels of cocaine ... solvent mixture of chloroform
and isopropanol or ethanol should be used. e simultaneous analysis can be made using
chloroform/isopropanol (9:1) or (3:1), and using columns of Bond Elut Certifyđ ... rmation of a target compound is usually achieved by agreement of its mass spectrum with
that of the authentic standard. Since, with simultaneous use of a deuterated IS, a mass
spectrum of a target...
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Drugs and Poisons in Humans - A Handbook of Practical Analysis (Part 23)
Ngày tải lên :
29/10/2013, 02:15
... 15 mg of free pentazocine. e solution is
transferred to a small glass centrifuge tube with a ground-in stopper, followed by addition of
several mg of solid K
2
CO
3
and 3 mL of chloroform. ... [5–7] and GC/MS [8]. In this chapter, a simple method for GC/MS analysis of
pentazocine in human whole blood and urine is presented.
Structures of pentazocine and dextromethorphan (IS).
⊡ Figure ... retention times of 3–7 min and 7–8 min, respectively. The amount of pentazocine
and IS spiked into 1 mL of blank whole blood or urine was equally 50 ng.
⊡ Figure 5.2
223
In two autopsy cases of pentazocine...
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The alchemy of meta-analysis
Ngày tải lên :
01/11/2013, 11:20
... stabilizer use or use of less proven agents).
Meta -analysis as interpretation
e above example demonstrates the dangers of meta -analysis, as well as some of its benets.
Ultimately, meta -analysis is not ... conict, the results of meta -analysis, despite the fanciness of
the word, should never be privileged over a large RCT. In the case of the example above, that
methodologically awed meta -analysis does ... The limits of statistics
probability of Y and a 25% probability of Z. But our brains cannot make out that dierence.
If this is correct, then “many of the techniques of statistical analysis that...
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Drugs and Poisons in Humans - A Handbook of Practical Analysis (Part 24)
Ngày tải lên :
08/11/2013, 01:15
... one of the most powerful hallucinogenic
drugs of abuse. LSD was explosively abused in U.S.A. in the latter half of the 1960s. In Japan,
the amount of seizure of LSD is much smaller than that of ...
of LSD was con rmed by Albert Hofmann who did synthesize the compound; the pharmaco-
logical activity can be obtained by oral administration of as small as 2075 àg of LSD. e ab-
sorption of ... manufacturers).
Developing solvents: (A) acetone/chloroform (4:1, v/v); (B) chloroform/methanol/n-hex-
ane (4:2:1, v/v).
Assessment of the method
e R
f
values of LSD were 0.29 with the (A) solvent system...
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Drugs and Poisons in Humans - A Handbook of Practical Analysis (Part 25)
Ngày tải lên :
08/11/2013, 01:15
... stream of nitrogen and recon-
stituted in 0.1 mL of DPM (IS) solution. A 1-àL aliquot of it is injected into the GC/MS
system with a DB-17MS system
k
.
Assessment of the methods
EI mass spectra of ... e
mass spectra of TFA derivatives of MDMA and its three metabolites obtained from the urine
specimen are shown in
> Fig. 7.5.
For the proof of the use of MDMA, detection of MDA along with ... with 2 mL of carbonate bu er solution (pH 10)
i
and extracted with 5 mL of chloroform/isopropanol (3:1, v/v).
234 3,4-Methylene dioxyamphetamines
Mass spectra of TFA derivatives of MDA, MDMA,...
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Drugs and Poisons in Humans - A Handbook of Practical Analysis (Part 26)
Ngày tải lên :
08/11/2013, 01:15
... Modification of EMIT assay reagents for improved sensitivity and cost effective-
ness in the analysis of hemolyzed whole blood. J Anal Toxicol 16: 381–388
7) Sneath TC, Jain NC (1992) Evaluation of phencyclidine ... utilizing the ETS
đ
analyzer and a 25-ng/
mL cutoff. J Anal Toxicol 16:107108
8) Diosi DT, Harvey DC (1993) Analysis of whole blood for drugs of abuse using EMIT d.a.u. reagents and a Mon-
arch ... of a whole blood or urine specimen.
ã 1 M NaHCO
3
solution: 8.4 g of NaHCO
3
is dissolved in distilled water to prepare 100 mL
solution.
ã Chloroform/methanol (9:1, v/v): a 100-mL volume of...
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