... strength and modulus ofmodified EPs A similar trend was found in the case of the tensile properties; the flexural strength and modulus ofmodified EPs are lower than those of the unmodified ... effect of CTBN content on the glass transition temperatures (Tg) of the EP Properties ofModified Epoxy Resin 3.3 Tensile Properties Table shows the effect of CTBN content on the tensile properties ... The effect of CTBN content and different testing speeds on the KIC of the EPs Properties ofModified Epoxy Resin In order to correlate the mechanical propertiesof the modified EP with morphology,...
... Bibliography 197 x List of Figures 1.1 Illustration of energy band structures of materials VB: valence band, CB: conduction band 1.2 Polaron and bipolaron structures of polythiophene ... Method and It's Applications 27 1.9 Propertiesand Characterization of Metal Nanoparticles 29 1.9.1 Solubility of Metal Nanoparticles 31 1.9.2 Size and Shape of Nanoparticles ... SYNTHESES AND SELF-ASSEMBLY OF NANOSTRUCTURE AS MODIFIEDELECTRODES FOR POLYTHIOPHENE PREPARATION ZHANG CHUNYAN (B Sc Nanjing University of P R China) A THESIS SUBMITTED FOR DOCTOR OF PHILOSOPHY...
... Izaki’s method, the incorporation of Zn into magnetite was finished by the deposition of magnetite film on ZnO thin film, so the Zn content of ferrite film and the magnetic properties cannot be well adjusted ... ions migrate to the surface of the Ag layer mediated by the electrostatic force, and the dehydration reaction is accompanied by the reactions of Eqs and The reduction of NOÀ ions to NOÀ ions is ... composed of fine Ag nano-granules of 1–10 nm in size The surface of the Ag layer possesses the large surface area of the fine Ag nano-granules Heterogeneous nucleation is promoted by the presence of...
... concentration of the SnCl4 solution, and the films were annealed at different temperatures and for different period of time Photoconductivity measurement In order to evaluate propertiesof obtained films ... steps of spray pyrolysis for TiO2 and sol-gel for SnO2 As prepared films exhibit a nanocomposite structure, constituting of a majority of TiO2 and a small amount of SnO2 located on the TiO2 grain ... Fundamental Research of Vietnam, Grant N 405606 References [1] N Castillo, D Olguin, A Conde- Gallardo, S Jiménez- Sandoval, Structural and morphological propertiesof TiO2 thin films prepared by...
... formation of SiO2 nanowires can obtained through XPS The two strong peaks at 103.35 and 532.65 eV as shown in Results and discussion TEM micrography shows the general morphology and dimension of SiONWs ... Fig 1(b) indicates the amoeba-shape of the nanowires, with the diameter of about 70 nm and a length up to tens of micrometers Fig 1(c) shows frog-egg morphology of the nanowires, which is similar ... tops of the nanowires [17] The growth of the nanowires Fig XPS of the sample (a) survey spectrum of the sample; (b) Si2p binding energy spectrum; (c) O1s binding energy spectrum Fig PL spectrum of...
... spectra of samples S2 (a) and S3 (b) can be exclusively indexed to ␣-Fe2 O3 , according to standard data (JCPDS 33-0664) In Fig 1(b) and (c), the reflection peaks of XRD patterns of S2 and S3, ... in sample S3 (e and f) B Lv et al / Particuology (2008) 334–339 and outer and inner diameters of 70–120 nm and 45–80 nm, respectively Fig 3(c) and (d) show the morphologies of Fe3 O4 nanotubes ... López-Urías, and Mu˜ oz-Sandoval (2005) n simulated the micromagnetic property of iron nanorings, and they found large coercive fields for din /dout > 0.5 (din and dout are the inner and outer diameters of...
... temperatures on the structural propertiesof the films has been investigated, and the optical propertiesof the films have also been analyzed Methods Synthesis ZnS films were deposited onto a Corning ... designed and carried out the experiments and wrote the first draft of the manuscript JHA analyzed the propertiesand helped draft the manuscript KNH and KSH detailed the original idea andmodified ... However, the FWHM value of the film prepared at 400°C increased to 0.154°, indicating the deterioration of the crystallinity of the films The mean crystallite sizes of the films were about 22.3,...
... measurements and the analysis of the spectra and carried out the analysis of the water contact angles on nanoporous alumina AK and CE participated in the design of the study and coordination of the ... of HMDS Page of with the alumina surface occurs by the dissociative chemisorption of HMDS via reaction of coordinatively unsaturated Al + and O-sites Subsequent reaction of pendant -O-SiMe3 and ... Figure 4) The wetting propertiesof unmodified thin film and nanoporous alumina surfaces were used as a reference Both unmodified alumina surfaces were wetted completely by water and, thus, they were...
... shown in Figure 2b, the bands of C-H and OCH2 are also observed in the surface -modified Cu nanoparticles, while the absorption peaks of P = S and P-S shifts, and the bands of N-H mostly disappear ... Netherlands) A Nexus 470 Fourier transform infrared spectrometer (NICOLET, USA) was employed to observe the changes of organic functional groups Preparationof nanofluids Three typesof nanofluids ... r and ν are the density and kinematic viscosity of the nanofluid, respectively, at the same temperature Measurements of the thermal conductivities of Cu nanofluids were performed by means of...
... frequency doubling and fast optical gating [11] and behaves as an X-ray detector [12] Electronic and optoelectronic propertiesof GaSe, GaS, and InSe materials indicate the possibilities of realizing ... well-established knowledge of the electrical and optical propertiesof GaSe thin films, in this paper, we report the results on electrical and optical measurements of amorphous thin films of GaSe nanorods ... diameter of the nanorods varies from 140 to 180 nm, and the length is of several hundreds of nanometers Figure presents the temperature dependence of the dc conductivity of thin films of a- GaxSe100-x...
... film-only properties In addition, a plot of Young’s modulus of ZnO thin films on three various substrates determined using the method of Oliver and Pharr [18] is illustrated in Fig 2(c) The variation of ... particular reference to the effects of substrates on mechanical propertiesof thin films/substrates systems Experimental Details The Growth Conditions of ZnO Thin Films ZnO thin films were grown on ... ð7Þ where Pmax and h(w) are denoted as the driving force and the displacement response of the indenter, respectively; U is the phase angle between Pmax and h(w); m is the mass of the indenter...
... characteristics of the MWNTs and overall morphology of the films are critical for FE This is also important because both structure and morphology of CNT films strongly depend on growth techniques and related ... motivation of the present study was to investigate the effect of substrate morphology on the growth of CNT films by an MPECVD process and investigate their comparative FE propertiesand structure–morphology ... Results and Discussion SEM micrographs of mechanically polished and the electrochemically etched Si wafers are shown in Fig 1a, b, respectively Randomly oriented pits of different shapes and size...
... to the range of normal TF (Table and Figure 1, 2) And the ratio of A260 to A280 was up to the criteria of National Health Department on transfer factor Contents of polypeptides and nucleotides ... lucidity Analysis of amino acids Three milliter of the sample of Specific and non-specific TF were added eight percent of Sulfonic-Salicylic acid for three milliter respectively and put at quiescence ... content of polypeptides in TF indicated that content of specific was higher than that of non-specific and was also closed to normal transfer factor sold on the store (Figure and Table 4) And the...
... morphology of the nanotube arrays is getting clear owing to the obvious thinning of the porous structure The pore diameter and the length of the nanotubes with roughness and ripples at the bottom of ... characteristic peaks of the as-anodized sample (Fig.6(a)) not arise from the TiO2 but from the conducting film (SnO2 and SnO) of Fig.6 XRD patterns of nanotublar TiO2/FTO electrodes annealed FTO and Ti, contributing ... Photoelectrochemical characterization of nanotubular TiO2/FTO electrodes Figs.7 and show the photocurrent response curves and electrochemical impedance spectra (EIS) of nanotubular TiO2/FTO electrodes annealed...
... resolution with some respect to FTIR spectroscopy and its versatility and simplicity in terms of sample handling, preparationand the possibility of acquisition of the whole spectra (4000 to 10 cm-1) with ... application of identification of compounds, there are a large number of reported works on the characterisation of concentration and mobility of free carriers, strain and crystal quality, determination of ... the lower edge of the O2p-like valence band and extend almost through the whole band Whereas, the uppermost valence band edge consists of pz-type states that form the lone pair (out -of- plane) π...
... tunable and pyroelectric propertiesof BZT thin films 1.2 The Scope of Thesis The aim of present research is to study the variations of microstructures and their correlations to the tunable and induced ... microstructures andpropertiesof BZT thin films observed from the increase in deposition temperature Td and annealing duration ta …………………………66 Table 5.1 Changes in microstructures andpropertiesof BZT ... encouragement, and understanding throughout my PhD candidature ii TABLE OF CONTENTS Title Page i Acknowledgments ii Table of Contents iii Summary of Thesis vii List of Table Captions ix List of Figure...
... the tunable and pyroelectric propertiesof the B-site doped BaTiO3, i.e., Ba(Ti1-xSnx)O3 (BTS) thin films The effects of stress and microstructure on the tunable propertiesof BTS thin films have ... high-quality growth template and effective diffusion barrier to reduce the dielectric loss and leakage current of the BTS films Improved tunable and pyroelectric propertiesof BTS films have been achieved ... dependence of P and FD of the BTS thin films at different applied electric fields (at 20 oC)……………………………………… 61 Table 5.1 Dielectric propertiesof BTS thin films buffered with BZN of different...
... Chapter and present the results and analysis, respectively, of the density changes in Cu-Zr and Zr-Cu-Al systems The measurement of Young’s moduli and coefficients of thermal expansion of amorphous ... of Young’s modulus and coefficients of thermal expansion of amorphous Cu-Zr thin films - 162 7.1 Measurement of Young’s modulus of amorphous Cu-Zr thin films - 162 7.1.1 ... elastic moduli and CTE of metallic glasses The contents of the thesis are arranged as follows: Chapter is a review of the fundamentals of phase-change materials and metallic glasses, and provides...