stability indicating hptlc determination of imatinib mesylate in bulk drug and pharmaceutical dosage

JOURNAL OF CHROMATOGRAPHY LIBRARY - VOLUME 24 chemical methods in gas chromatography

JOURNAL OF CHROMATOGRAPHY LIBRARY - VOLUME 24 chemical methods in gas chromatography

Ngày tải lên : 06/10/2016, 09:25
... 9.5.3 Determination of main oxygen-containing groups 9.5.4 Determination of some sulphur-containing groups 9.5.5 Determination of alkoxy groups ... identification and group determination of components in complex mixtures of compounds, to improve separation and to enhance the sensitivity and, in some instances, the accuracy of determination of sample ... biologically interesting amino acids; C, some amino acids in the presence of protein amino acids A: ALA = alanine; GLY = glycine; VAL = valaine; THR = threonine; SER = serine; LEU = leucine; ILE...
  • 329
  • 732
  • 0
mathematical methods of engineering analysis - e. cinlar, r. vanderbei

mathematical methods of engineering analysis - e. cinlar, r. vanderbei

Ngày tải lên : 31/03/2014, 15:21
... compactness and convergence 11.5 DEFINITION A point x in E is called a cluster point of a subset A of E provided that every open ball centered at x contains in nitely many points of A 11.6 THEOREM ... finte number of them that cover C and, therefore, A Since each one of those finitely many balls has a finte number of points of A, the total number of points in A must be finite The following is the ... corresponding metrics d, d , etc Given a mapping T from E into E , we write T x for the image of the point x of E and T −1 B for the inverse image of the subset B of E On a first reading, the...
  • 119
  • 395
  • 0
MATRIX METHODS OF CIRCULAR ANALYSIS

MATRIX METHODS OF CIRCULAR ANALYSIS

Ngày tải lên : 08/04/2014, 11:28
... Element 2-3 Substitutingv,, e,, v, ando, into equations (23.70 )and (23.72) ,and remembering that the first node is node and the second node is node 3, the following is obtained for M, and M,: = M, -1.152 ... principle of superposition: Fix the beam at its nodes and determine the end furing forces, as shown in the following figure at (a) and (b) and as calculated below The beam in condition (1) is not in ... which in this case is u , and u2 {R} = a vector of reactions corresponding to the constrained displacements, which in this case is u3 [K,J in this case = WI21= [o - E2 I , ] [ -i E2 / Expanding...
  • 62
  • 375
  • 0
methods of behavior analysis in neuroscience - jerry j. buccafusco

methods of behavior analysis in neuroscience - jerry j. buccafusco

Ngày tải lên : 08/04/2014, 12:37
... presenting and grooming This preoccupation with presenting and grooming by the stump-tailed monkeys resulted in lower scores in the remaining behavioral categories The reports of Kling and Orbach51 ... were interested in the estrous cycle of the rat To support their research interests, Long and Evans established one of the leading strains of rats that continues to bear their names The origins of ... impaired in ability to perform learning and memory-related tasks and exhibit a decrease in the expression and nicotine-stimulated function of brain nicotinic acetylcholine receptors These cholinergic...
  • 329
  • 4.4K
  • 0
Statistical Methods of Valuation and Risk Assessment: Empirical Analysis of Equity Markets and Hedge Fund Strategies

Statistical Methods of Valuation and Risk Assessment: Empirical Analysis of Equity Markets and Hedge Fund Strategies

Ngày tải lên : 16/04/2013, 20:00
... 49 -3- Introduction Much of the financial decision making by financial institutions is focuses on risk management Measuring risk and analysing ways of controlling and allocating it require ... individuals and institutions desiring to make investment decisions involving hedge funds A detailed analysis of hedge fund risks and returns is also important from the standpoint of asset pricing theory ... - Index and the Goldman Sachs Commodity Index We also include CSFB High Yield index to incorporate returns available from investing in high yield securities Finally we include the volatility index...
  • 59
  • 476
  • 0
trace analysis technology of nenophenyl in wastewater analysis by  GCMS

trace analysis technology of nenophenyl in wastewater analysis by GCMS

Ngày tải lên : 16/03/2014, 18:11
... method was examined in terms of its practicability for the determination of the three components in the sewage in uents and effluents of wetland plants In addition, the applicability of the SPME–GC– ... for t-NP and BPA and 2% for EE, and was completely prevented by keeping the fibre in the PTV-injector (split mode) for The LODs determined in pure water and wastewater samples (effluent and model ... signal-to-noise ratio of about 3:1 The LODs of the EDs in pure water were appointed with blank values and lower calibration levels used for the determination of the linear range and were found to...
  • 11
  • 463
  • 0
Methods of analysis of food components and additives

Methods of analysis of food components and additives

Ngày tải lên : 23/05/2014, 12:30
... cell cell determination of tota l parameters: determination of total parameters: V OC, POC, V OX POX VOC, POC, VOX, ,POX individual determination of compound s individual determination of compounds ... University of Szczecin Szczecin, Poland Malgorzata Michalska Institute of Maritime and Tropical Medicine Gdynia, Poland Keith A Lampel U.S Food and Drug Administration Laurel, Maryland Robert ... gamut of food components, including antioxidants, aroma compounds, carbohydrates, drug residues, lipids, peptides and proteins, toxins, and vitamins A summary of developments in the use of MS in...
  • 436
  • 1.3K
  • 0
direct methods for stability analysis of electric power systems theoretical foundation, bcu methodologies, and applications

direct methods for stability analysis of electric power systems theoretical foundation, bcu methodologies, and applications

Ngày tải lên : 30/05/2014, 23:38
... Indeed, the problem of determining stability regions (regions of attraction) of nonlinear dynamical systems is of fundamental importance for many disciplines in engineering and in the sciences (Athay ... concepts used in the literature Stability is a very broad subject, and the concept of stability can be formulated in a variety of ways depending on the intended use of stability analysis and design ... the question of stability of ¯ (t) involves the following two steps: x Determine if the y = solution of Equation 3.5 is stable Show that stability (or instability) of the y = solution of Equation...
  • 511
  • 1.2K
  • 0
Báo cáo nghiên cứu khoa học: " EXPERIMENTAL AND THEORETICAL ANALYSIS OF A CRITICAL CHEMICAL REACTION: DECOMPOSITION OF HYDROGEN PEROXIDE (H2O2)" potx

Báo cáo nghiên cứu khoa học: " EXPERIMENTAL AND THEORETICAL ANALYSIS OF A CRITICAL CHEMICAL REACTION: DECOMPOSITION OF HYDROGEN PEROXIDE (H2O2)" potx

Ngày tải lên : 22/07/2014, 03:20
... regarding safety aspects 2.2 Kinetics of the decomposition of hydrogen peroxide In the case of the decomposition of hydrogen peroxide, the reaction is regarded as irreversible, since one of the ... change in kinetics and potential energies, and that all heat fluxes and the shaft work are zero except for the heat fluxes respective to the reaction and to the cooling d (ρVr H ) & & & & = Vin ρHin ... performed are summarized in table (1) The influences of hydrogen peroxide and catalyst concentration and of the initial temperature of the reactor on the reaction rate and the heat flow behavior...
  • 9
  • 463
  • 0
Báo cáo vật lý: "Analysis of Trace Elements in Teeth by ICP-MS: Implications for Caries" pptx

Báo cáo vật lý: "Analysis of Trace Elements in Teeth by ICP-MS: Implications for Caries" pptx

Ngày tải lên : 07/08/2014, 14:20
... techniques, including the use of microprobes Our results indicate that trace elements are systematically but inhomogeneously distributed within the enamel and dentine of teeth.10 Sources of Cd include ... smelting, and disposal of metal waste Other sources include the use of Cd for industrial applications, such as in the production of pigments, stabilisers, and alloys In addition, Cd is present in ... to determine how the major components of the amalgam (Cu, Zn and Hg) diffuse into the structures of the teeth Curson and Crocker20 determined the concentrations of Zn and Pb in the pulp of the...
  • 12
  • 429
  • 0
Soil Sampling and Methods of Analysis - Part 2 ppt

Soil Sampling and Methods of Analysis - Part 2 ppt

Ngày tải lên : 12/08/2014, 02:23
... analyzing tree nursery and forest soils often determine both NO3 and NH4 There is considerable diversity among laboratories in the extraction and determination of NO3 and NH4 In addition, incubation ... aeolian sand The findings of Doyle and Fletcher (1977) pointed to the potential usefulness of information on the Se content of soil parent materials when designing sampling programs for investigating ... Standard solution for Cu, Zn, and Mn determination by atomic absorption: a Combined Cu and Zn standard solution: 0, 0.2, 0.4, 0.8, 1.2 to 2.0 mg mLÀ1 of Cu and of Zn in M3 extractant b Mn standard...
  • 104
  • 768
  • 2
Soil Sampling and Methods of Analysis - Part 5 ppt

Soil Sampling and Methods of Analysis - Part 5 ppt

Ngày tải lên : 12/08/2014, 02:23
... present in any solution, including soil extracts This might explain the confusion perceived in the scientific literature pertaining to the definition of soil DOM A clear definition and distinction ... weight equivalent) into jars and record the weight of each jar plus soil without its lid Place one vial containing 10 mL of M NaOH and one vial containing water into each jar and seal them with ... POTENTIALLY MINERALIZABLE N 46.2.1 THEORY In theory, potentially mineralizable N is the amount of N that will mineralize in infinite time at optimum temperature and moisture It is estimated by incubating...
  • 126
  • 1.7K
  • 1
Soil Sampling and Methods of Analysis - Part 7 pot

Soil Sampling and Methods of Analysis - Part 7 pot

Ngày tải lên : 12/08/2014, 02:23
... profile The zone of influence of the EM field in the metal ring probes includes the plastic separating the rings, the PVC access pipe, and the surrounding soil, which is in a fringe field of ... without structure (loam) Figure 69.7a; and generally speaking, a(c0 ) increases as c0 increases, indicating an increase in the importance of the gravity component of infiltration relative to the capillarity ... of Æ0:01 m3 mÀ3 The EM field for TDR measurement propagates both in the resin comprising the probe, and in the surrounding soil, with more of the field in soil in wet than in dry soil, meaning...
  • 282
  • 905
  • 0
Soil Sampling and Methods of Analysis - Part 8 (end) pdf

Soil Sampling and Methods of Analysis - Part 8 (end) pdf

Ngày tải lên : 12/08/2014, 02:23
... contamination of these organisms, including direct skin contact, inhalation, or ingestion All bacteria, including transgenic lines (e.g., carrying an antibiotic resistance gene), must be maintained ... eye injury Skin contact: Causes skin burns May cause deep, penetrating ulcers of the skin Ingestion: Causes gastrointestinal tract burns May cause perforation of the digestive tract Bases and ... eye injury Skin contact: Causes skin burns May cause deep, penetrating ulcers of the skin Ingestion: Causes gastrointestinal tract burns May cause perforation of the digestive tract Does not induce...
  • 12
  • 289
  • 0
Báo cáo y học: "Application of methods of identifying receptor binding models and analysis of parameters" potx

Báo cáo y học: "Application of methods of identifying receptor binding models and analysis of parameters" potx

Ngày tải lên : 13/08/2014, 22:22
... because of experimental errors and/ or receptor binding complexity [9,10] In particular, graphic methods are inapplicable for definition of the cooperative binding parameters and for analysis of non-equilibrium ... explored for discriminating among models for receptor binding model and for defining the relevant parameters The procedure devised allows one to determine the receptor binding model and its parameters, ... Biology and Medical Modelling 2004, 1:11 Interaction of one ligand with N types of binding sites k+ j  → Rj + L R L; j = 1, N ← j  k− j ( 3) Let us note that the ligand-receptor interaction...
  • 4
  • 290
  • 0
Báo cáo sinh học: "Reaction norms of size characters in relation to growth temperature in Drosophila melanogaster: an isofemale lines analysis" ppsx

Báo cáo sinh học: "Reaction norms of size characters in relation to growth temperature in Drosophila melanogaster: an isofemale lines analysis" ppsx

Ngày tải lên : 14/08/2014, 19:22
... we often include simultaneous analyses concerning wing, thorax and ratio, in order to save space Data included in the tables but concerning the ratio is discussed in the second section Wing and ... allow an increase of the wing loading, ie the weight per surface unit of the wing In preliminary experiments, we measured the wing loading of males grown at temperatures, ie 12, 21 and 30°C: ... The isofemale line heritability of the ratio is high, comparable to that of the wing and superior to that of the thorax DISCUSSION As pointed out in the Introduction, numerous observations and...
  • 23
  • 203
  • 0
a comparative analysis of methods of defense against buffer overflow attacks

a comparative analysis of methods of defense against buffer overflow attacks

Ngày tải lên : 18/10/2014, 18:09
... payload string cannot contain the null character since this would abort the copying of the payload into the buffer Some copying routines of the C library use carriage returns and new lines as a ... processing of strings But at the same time it is also dangerous, because the scheme breaks down if a string is not null terminated, and because there is no way of knowing the length of the string ... scrutinize the software but relatively uncoordinated The latter is characteristic of commercial organizations, with fewer pairs of eyes scrutinizing the software but in a much more systematic and...
  • 16
  • 341
  • 0
Novel methods for quantitative analysis and evaluation of effects of chronic exposure to microcystins by capillary electrophoresis and metabolomic studies

Novel methods for quantitative analysis and evaluation of effects of chronic exposure to microcystins by capillary electrophoresis and metabolomic studies

Ngày tải lên : 11/09/2015, 10:14
... (protein) amino acids which can be leucine (L) and arginine (R) in microcystin LR, arginine (R) and arginine (R) in microcystin RR, Leucine (L) and tryosine (Y) in microcystin LY etc Microcystins ... cylindrospermopsin and neurotoxins such as anatoxin-a, anatoxin-a(s) and saxitoxins, the marine toxin aplysiatoxin, debromoaplysiatoxin and lyngbyatoxin-a), and lipopolysaccharides (LPS) All are biotoxins ... microcystins, nodularin and cylindrospermopsin) in water and potential effects of exposure to microcystins were investigated The effect of exposure of a human cell line to low amounts of microcystins...
  • 177
  • 292
  • 0
Instrumental methods of analysis

Instrumental methods of analysis

Ngày tải lên : 01/12/2015, 22:43
... and in pollution monitoring 3.It is extensively used in determination of alkali and alkaline earth metals in soil,glass,ceramic,cement etc., 5.15.4 DETERMINATION OF CONCENTRATION OF SODIUM AND ... Complex ion determination (iv) Determination of percentages of keto and enol forms (v) Determination of ozone level in atmosphere (λ260nm) (vi) Study of cis & trans isomers (vii) Study of H+ ion ... Clinical Chemistry : : To analyse metals in water and waste water Determination of total serum protein, serum (iii).Industrial Chemistry: Cholesterol, etc industry pharmaceuticals, food, paint,...
  • 21
  • 412
  • 0
Otles methods of analysis of food components and additives

Otles methods of analysis of food components and additives

Ngày tải lên : 02/12/2016, 12:54
... University of Szczecin Szczecin, Poland Malgorzata Michalska Institute of Maritime and Tropical Medicine Gdynia, Poland Keith A Lampel U.S Food and Drug Administration Laurel, Maryland Robert ... gamut of food components, including antioxidants, aroma compounds, carbohydrates, drug residues, lipids, peptides and proteins, toxins, and vitamins A summary of developments in the use of MS in ... retention trap, narrowing chromatographic bands of the analytes The sample volume during fast injection spreads in the column inlet, flooding it and causing “band broadening in the space,” so it...
  • 451
  • 387
  • 0