4 new trends and future developments of platinum based antitumor drugs
báo cáo hóa học: " Robot-assisted reaching exercise promotes arm movement recovery in chronic hemiparetic stroke: a randomized controlled pilot study" pptx
... Activeassist Supported FS 12 24 12 24 12 24 12 24 12 24 12 24 Moderate 12 24 12 24 12 24 12 24 Severe 12 24 12 24 12 24 12 24 12 24 12 24 Free Reaching Moderate 12 24 12 24 12 24 Session number Figure ... 0.2 (0 .4) Free reaching 3.2 (1.0) 0.3 (0.5) Active-assist 16 .49 ( 14. 5) -6.28 (11 .48 ) Free reaching 10 .44 (6.0) 0 .47 0 -0.085 (0.25) Active-assist 0. 246 -0.108 (0.18) Free reaching 0 .41 4 0.0 24 (0.07) ... (1.0) 55.9 (10.5) 8 /4 99.2 (47 .9) 9/3 2.7 (0.5) 55 .4 ( 14. 9) 3 /4 71.3 (45 .0) 5/2 4. 3 (0.5) Free reaching trained 5/5 Robot trained 75.8 (45 .5) 55.9 (12.3) Free reaching trained 4/ 6 Robot trained...
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Báo cáo y học: "Effect of Acute Administration of an Herbal Preparation on Blood Pressure and Heart Rate in Humans"
... ±9.7 0. 84 ±0.06 PL post 63 .4 ±13.1 117.9±12.7 78.1 ±8.2 91.3 ±8.9 0. 84 ±0. 04 DS pre 65.8 (15.2 64. 7 (13.7 119 .4 13.6 77.9 ±9.2 120.6±11.1 80.6 ±6.3 91.8 ±10.3 94. 0 ±7.3 0. 84 ±0.05 0.81 ±0. 04* 60.9 ... 52 mg p-synephrine and 7 04 mg caffeine over a 24 hour period Table Subject characteristics Overall Females (n= 14) Males (n=9) Age (yrs) 24. 5 ± 7 .4 25 .4 ± 9.3 Height (m) 1. 74 ± 0.09 1.68 ± 0.07 ... decongestants and is not a constituent of C aurantium Because of the known cardiovascular effects of nor-epinephrine and ephedrine, it has generally been assumed that consumption of p-synephrine and bitter...
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Improvement of nutrient removal and phosphorus recovery in the anaerobic/oxic/anoxic process combined with sludge ozonation and phosphorus adsorption
... into the system The characteristics of the influent wastewater were as follows: 160–200 mg/L of SS, 55–80 mg/L of TOC, 45 –55 mg/L of T-N, and 4. 0–5.5 mg/L of T-P In this study, four different ... removal and denitrification (3) Most of the phosphorus in the sludge was solubilized by ozonation, and a large part of the solubilized phosphorus consisted of PO4-P Over 90% of the PO4-P was ... T-P concentrations in the effluent and MLSS in the reactor Figure shows the water quality profiles at day 49 (Phase 2), day 78 (Phase 3), and day 147 (Phase 4) In Phase 2, the effluent T-N concentration...
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Drugs and Poisons in Humans - A Handbook of Practical Analysis (Part 17)
... of 0 .4 mL of blank blood and 0 .4 mL of IS- containing pentane solution in a glass vial with a Teflon-septum screw cap, which has been cooled with ice, and vortex-mixed for s; a 3-µL aliquot of ... Assessment and some comments on the method > Figure 8.1 shows gas chromatograms of isobutyl nitrite (injected amount µg) and isobutyl alcohol (injected amount 10 µg); they appeared at 3 .4 and 7 .4 of ... detection limits of isobutyl nitrite and isobutyl alcohol in liquid specimens were 62 ng and 1.9 µg/mL, respectively [7] > Figure 8.2 shows EI mass spectra of isobutyl nitrite (A) and isobutyl alcohol...
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Drugs and Poisons in Humans - A Handbook of Practical Analysis (Part 67)
... Trace Analysis of Chemical Warfare Agents An Approach to the Environmental Monitoring of Nerve Agents Ministry of Foreign Affairs of Finland, Helsinki, pp 27, 28, 37–39, 59– 64, 72–79 and 90–99 2) ... examine the coexistence of VX and DAEMS by SIM measurements at m/z 1 14 625 626 VX and its decomposition products In the mass spectrum of DAEMS, other fragment ions at m/z 72,128 and 75, due to [(iPr)N ... analysis of DAEMS, various concentrations of DAEMS are spiked into blank serum specimens containing a fixed amount of DAEMO (IS) each and extracted as described before Since the base peaks of DAEMS and...
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Drugs and Poisons in Humans - A Handbook of Practical Analysis (Part 20)
... 5α-cholestane 372 372 5’-nor-∆8-THC -4 -ioc acid 47 4 41 6, 333 ⊡ Figure 2 .4 Mass spectra of the methyl ester plus TMS and TMS derivatives of ∆9-THC-11-oic acid The Substance Abuse and Mental Service Administration ... 14) Yamamoto I (1992) Methods for analysis of cannabis and its components In: The Pharmaceutical Society of Japan (ed) Standard Methods of Chemical Analysis in Poisoning – With Commentaries, 4th ... acid, 5α-cholestane and 5’-nor-∆8-THC -4 -ioc acid with different derivatizations Derivatization-1 Derivatization-2 Diagnostic ion (m/z) ∆9-THC-11-ioc acid 48 8, 47 3, 371 43 0, 41 5, 371 5α-cholestane...
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Drugs and Poisons in Humans - A Handbook of Practical Analysis (Part 21)
... Therefore, the detection of low levels of morphine starting from a large amount of a specimen cannot be a proof of the intake of the drug The level of morphine in urine of healthy subjects determined ... intake [4] HPLC analysis Reagents and their preparation • • Standard solutions of morphine for a calibration curve (2, and 20 µg/mL): see “Reagents and their preparation”, above of GC and GC/MS ... analysis is made by the comparison of the retention time of a peak of a specimen with that of the authentic standard and also by the confirmation of the absence of such a peak in a blank specimen...
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Drugs and Poisons in Humans - A Handbook of Practical Analysis (Part 70)
... volume of the supernatant solution is transferred to a new polypropylene tube of the same type, followed by addition of 0.5 mL of concentrated sulfuric acid f and 0.5 mL of mesitylene Nitrate and ... addition of 20 mg of anhydrous sodium carbonate and vortex-mixed for After centrifugation at 3,000 rpm for min, 1- or 4- µL of the upper layer is injected into GC Various known amounts of nitrate and ... He; flow rate: 2.1 mL/min Procedures i Analysis of nitrate i ii iii iv v vi A 0.2-mL volume of a test specimen, 20 µL of IS solution and 0.2 mL of the saturated silver acetate solution e are placed...
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Drugs and Poisons in Humans - A Handbook of Practical Analysis (Part 71 and End)
... 265, 271, 2 74, 283, 3 04, 317, 331, 371, 373, 3 74, 40 8, 41 7, 42 7, 43 7, 44 3, 44 4, 44 9, 45 6, 47 8, 48 3, 49 9, 509, 511, 527, 536, 545 , 563, 5 84, 585, 600, 602, 610, 611, 620, 631 GC/MS/MS 41 , 85 gentisic ... hypaconine 46 1 hypaconitine 45 5, 45 9 hypersil 311 hypochlorite 40 3, 40 4 I ibuprofen 325, 330, 332, 333 IC 39 IC-A15 638 IC/ICP-MS 638, 641 ICP 41 , 42 ICP-AES 638, 644 ICP-MS 41 , 638 illudin S 47 4 imipramine ... acetylsalicylic acid 343 , 344 , 346 , 348 , 392 acid 187, 377 acidosis 123 aconine 45 8, 46 1 aconite toxins 45 5 aconitine 45 5, 45 8, 45 9 aconitum alkaloids 45 5 acylation 30 adhesives 149 adulterant 49 1 advanced...
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Drugs and Poisons in Humans - A Handbook of Practical Analysis (Part 22)
... Cocaine 19 .4 (0.06) 81.5 (0.27) 7 64 (2.52) 82 .4 (0.27) 41 .1 (0. 14) 103 (0. 34) 44 (0.15) 148 (0 .49 ) 171 (0.56) 109 (0.36) 71.3 (0. 24) 655 (2.16) EME 30.9 (0.16) 242 (1.22) 66 (0.33) 47 (0. 24) 2.9 ... amounts of unchanged cocaine, EME and BE excreted into urine are 1– 14 %, 12–60 % and 14 55 % of total amount of cocaine administered, respectively [16, 18, 19] Because of the basicity of cocaine, ... 28.5 (0. 14) 6.1 (0.03) 32 .4 (0.16) 41 .5 (0.21) 51.1 (0.26) 25.9 (0.13) 30.7 (0.15) BE 28.5 (0.01) 48 7 (1.69) 155 (0. 54) 20.3 (0.07) 5.8 (0.02) 41 .5 (0. 14) 5.1 (0.02) 23.0 (0.08) 160 (0.55) 46 .3 (0.16)...
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Drugs and Poisons in Humans - A Handbook of Practical Analysis (Part 23)
... its concentrations were 9.2 and 3.3 µg/mL in blood, 43 and 34 µg/g in the liver, and not detectable and 4. 5 µg/mL in urine, respectively [12] The blood concentrations of dextromethorphan, which ... history of intravenous use of pentazocine and tripelennamine, T,s and Blues J Forensic Sci 28 :48 9 49 5 3) Kintz P, Tracqui A, Lugnier AJ et al (1990) Simultaneous screening and quantification of several ... Determination of pentazocine in human plasma by high performance liquid chromatography Pharmazie 46 :46 4 46 5 8) Seno H, Kumazawa T, Ishii A et al (2000) Determination of pentazocine in human whole blood and...
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Drugs and Poisons in Humans - A Handbook of Practical Analysis (Part 24)
... Darmstadt, Germany and other manufacturers) Developing solvents: (A) acetone/chloroform (4: 1, v/v); (B) chloroform/methanol/n-hexane (4: 2:1, v/v) Assessment of the method The Rf values of LSD were 0.29 ... (1992) Standard Methods of Chemical Analysis in Poisoning – With Commentary – Nanzando, Tokyo, p 43 and p 151 (in Japanese) 3) Cody JT (2000) Hallucinogens In: Bogusz MJ (ed) Handbook of Analytical ... about 10 µg and LSD is rapidly metabolized in human bodies As metabolites of LSD, 2-oxo-LSD, 3-, 13- and 14- hydroxy-LSDs and an N-de-ethyl-LSD are known [3] After oral ingestion of 160 µg LSD,...
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Drugs and Poisons in Humans - A Handbook of Practical Analysis (Part 25)
... procedures for GC/MS and LC/MS analyses of MDAs in the forms of tablets and those for GC/MS analysis of MDAs and their main metabolites 4- hydroxy-3-methoxymethamphetamine (HMMA) and 4- hydroxy-3-methoxyamphetamine ... (MDMA) and its metabolites in plasma and urine by HPLC-DAD and GC-MS J Anal Toxicol 20 :43 2 44 0 7) Ortuño J, Pizarro N, Farré M et al (1999) Quantification of 3 ,4- methylenedioxymethamphetamine and ... For the proof of the use of MDMA, detection of MDA along with MDMA itself is being usually performed [12– 14] However, the main metabolic pathway of MDMA in humans is the 233 2 34 3 ,4- Methylenedioxyamphetamines...
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Drugs and Poisons in Humans - A Handbook of Practical Analysis (Part 26)
... mass spectra of PCP and pethidine (IS) Compound PCP IS m/z (% peak intensitiy) 200 (100) 242 ( 84) 246 (100) 71 (98) 84 ( 24) 172 ( 84) 91 (18) 232 (63) 186 (13) 218 (46 ) Assessment of the method ... fluorescence Clin Chem 40 :1819–1822 23) Schulz M, Schmoldt A (2003) Therapeutic and toxic blood concentrations of more than 800 drugs and other xenobiotics Pharmazie 58 :44 7 47 4 24) Jackson JE (1989) ... Disposition of Toxic Drugs and Chemicals in Man, 6th edn Biomedical Publications, Foster City, pp 47 2 47 5 14) Helrich M, McAslan TC, Skolniks S et al (19 64) Correlation of blood levels of 4- hydroxybutyrate...
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Tài liệu Drugs and Poisons in Humans - A Handbook of Practical Analysis (Part 27) ppt
... 19:591–5 94 5) Ishikawa Y, Suzuki O, Hattori H (1990) Positive -and negative-ion mass spectrometry and rapid clean-up of 19 phenothiazines Forensic Sci Int 44 :93–105 6) The Pharmaceutical Society of ... amount of IS and various concentrations of a target compound are added to mL each of blank whole blood or urine, and processed as above At least vials containing different concentrations of the ... Assessment of the method > Figure 1.1 shows a TIC and MCs for phenothiazine drugs obtained by GC/MS Panels A and B show a TIC and an MC for the authentic compounds, respectively; panels C and D those...
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Tài liệu Drugs and Poisons in Humans - A Handbook of Practical Analysis (Part 28) pptx
... in 0.1 mL of the mobile phase of HPLC or LC/MS For HPLC-DAD and LC/MS, 50 and 20 µL of the above solution are injected, respectively For the SIM of LC/MS, the ions at m/z 376, 378 and 42 2 are used ... RHP; m/z 42 2 .4: BP=IS Poisoning cases, and toxic and fatal concentrations Notes a) When GC/MS, HPLC and LC/MS are compared for analysis of haloperidol and bromperidol, the LC/MS seems of the best ... reported to be 5 40 and 50–100 ng/ mL, respectively; therapeutic blood levels of bromperidol 2–20 ng/mL [19] Therapeutic and toxic blood levels of floropipamide were reported to be 0.1–0 .4 and 0.5–0.6...
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Tài liệu Drugs and Poisons in Humans - A Handbook of Practical Analysis (Part 29) ppt
... detection of the peak of lofepramine Poisoning cases, and toxic and fatal concentrations In > Table 3.1, the therapeutic and toxic blood concentrations of each compound are shown [4] For all drugs, ... 0 .49 1.38 0.53 1.00 iii 1.32 0 .45 1.92 0.52 1.00 v 1.35 0 .45 1.60 0.56 1.00 vi 1.22 0 .41 1 .45 0 .41 1.00 vii 1. 24 0.66 1 .45 0.53 1.00 (15.195 min) ( 24. 237 min) ( 14. 003 min) (38.997 min) (18.687 ... a new reversed-phase chromatographic column of mm porous micropherical silica gel J Chromatogr B 692 :40 5 41 2 4) Baselt RC, Cravey RH (1995) Disposition of Toxic Drugs and Chemicals in Man, 4th...
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Tài liệu Drugs and Poisons in Humans - A Handbook of Practical Analysis (Part 30) doc
... 382 (100), 326 (87), 341 (63), 353 (33), 156 (31) 342 (100), 344 (47 ), 313 (37), 266 (31), 125 ( 24) 313 (100), 315 (76), 238 (71), 75 (62), 342 (52) 3 94 (100), 392 (77), 245 (43 ), 118 (38), 123 ... intensity) 207 (100), 242 (91), 244 (30), 270 (20),165 (15) 2 74 (100), 301 (96), 302 (92), 109 (43 ), 283 (37) 283 (100), 256 ( 94) , 2 84 (88), 221 (36), 110 (31) 242 (100), 270 (69), 103 ( 34) , 89 (33), 76 ... (100), 253 (95), 2 34 (80), 2 64 (61), 206 (58) 280 (100), 3 14 (87), 315 (68), 288 ( 54) , 89 (52) 259 (100), 293 (65), 2 94 ( 64) , 205 (59), 89 (50) 279 (100), 273 (90), 308 (88), 2 04 ( 84) , 102 (82) 382...
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Tài liệu Drugs and Poisons in Humans - A Handbook of Practical Analysis (Part 31) ppt
... Matsubara et al [ 14] , and 31.5 and 40 .8 µg/mL by Yashiki et al [15] Poisoning cases Many cases of poisoning by bromisovalum were reported In this section, representative clinical and medicolegal ... were: height, 151 cm; weight, 49 kg; mild subcutaneous hemorrhages observable in the chest, abdomen and extremities; and lung edema (left lung 46 0 g, right lung 44 0 g) Except these findings, neither ... stomach contents consisted of 14 g of white clayey substance and about 350 mL of aqueous solution About 350 mL urine was present in her urinary bladder Analytical results: g of bromisovalum was detected...
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Tài liệu Drugs and Poisons in Humans - A Handbook of Practical Analysis (Part 32) ppt
... 235 218 232 2 04 232 207 235 1 84 172 170, 112, 169 1 84, 126, 112 1 24, 80, 141 , 106, 53 138, 1 94, 110, 221 141 , 157, 55, 98 1 84, 112, 126 156, 157, 55, 98 1 84, 112, 126 168, 97, 1 24, 55 195, 181, ... 12 .4 12 .4 Detection limit (pg/on-column) 139 52 667 46 667 61 667 60 43 5 48 169 52 306 57 1,670 57 1,360 89 80 Calibration curves: 10, 25, 50, 100, 500 and 1,000 µL of the standard solution of ... 1 42 4. 2–1 34 Toxic conc Fatal conc Reference 10–30 >9 >5 >8 40 – 60 4 90 >7 13–96 9–72 10–169 8–73 >80 4 120 10 40 0 6–392 [18] [19] [18] [19] [18] [19] [18] [19] 309 310 Barbiturates Survived and...
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- small and medium enterprises in malaysia new challenges and future research
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- 1 medicinal inorganic chemistry state of the art new trends and a vision of the future
- 3 current status and mechanism of action of platinum based anticancer drugs
- tolerance amp mdash state of the art and future developments
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