1 medicinal inorganic chemistry state of the art new trends and a vision of the future

báo cáo hóa học: " Robot-assisted reaching exercise promotes arm movement recovery in chronic hemiparetic stroke: a randomized controlled pilot study" pptx

Ngày tải lên : 19/06/2014, 10:20

... actuates a hand piece and forearm trough (T) attached to a user's arm (A) back and forth along a linear track A sixaxis force sensor (F) measures the interaction forces between the user and the ... statically counterbalanced so that it does not gravitationally load the arm The hand piece consists of a trough for the forearm and a cm diameter cylinder placed in the palm of the user's hand ... the outpatient population at the Rehabilitation Institute of Chicago and from a participant database (Table 1) A power analysis indicated that with ten subjects in each group there would be a...

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Báo cáo y học: "Effect of Acute Administration of an Herbal Preparation on Blood Pressure and Heart Rate in Humans"

Ngày tải lên : 25/10/2012, 11:10

... (ANOVA) For the first data analysis, treatment and time were the independent factors using all 23 subjects The second analysis separated and analyzed the data according to gender The third analysis ... cardiovascular effects of C aurantium has been due, at least in part, to a lack of understanding of the differences in the pharmacokinetic and pharmacological properties between p-synephrine and ... breakpoint of 15 0 mg caffeine per day to separate the two groups Statistical significance was established at p

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Improvement of nutrient removal and phosphorus recovery in the anaerobic/oxic/anoxic process combined with sludge ozonation and phosphorus adsorption

Ngày tải lên : 05/09/2013, 09:38

... et al., 2008; Cui and Jahng, 2004; Kamiya and Hirotsuji, 19 98; Nagare et al., 2008; Sakai et al., 19 97; Saktaywin et al., 2005; Suzuki et al., 2006; Yasui et al., 19 96; Yasui and Shibata, 19 94) ... adsorption column and the backwash water, was circulated back to the anaerobic tank and the oxic tank at an appropriate rate (Table 1) Table Operational conditions The hydraulic retention time ... (Fig 1B) During 15 2 days operation of a lab-scale reactor, the operational conditions were optimized by changing the amount of sludge to be ozonated and the recirculation ratio of the residual...

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Drugs and Poisons in Humans - A Handbook of Practical Analysis (Part 17)

Ngày tải lên : 18/10/2013, 00:15

... concentration of an alkyl nitrite on the horizontal axis and peak area on the vertical axis The concentration of the analyte in a specimen is calculated using the calibration curve i Assessment and some ... with a 25 G × 1 needle (0.50 × 25 mm, Terumo, Tokyo, Japan and other manufacturers) and rapidly injected into GC iv Quantitation: a 0.25 mL of the same matrix e (without an analyte), 0.5 mL of the ... injection to GC, and from the standard solution to a test specimen) In principle, the sampling, extraction and GC analysis should be made at low temperature, in a gastight state and in a short time...

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Drugs and Poisons in Humans - A Handbook of Practical Analysis (Part 67)

Ngày tải lên : 18/10/2013, 00:15

... (a) a TIC and mass chromatograms; (b) an EI mass spectrum of the t-BDMS derivative of EMPA; (c) a CI mass spectrum of the same derivative of EMPA data of animals According to the reports by the ... GC/MS analysis for DAEMS in serum (a) a total ion chromatogram (TIC) and a mass chromatogram; (b) an EI mass spectrum of DAEMS; (c) a CI mass spectrum of DAEMS Poisoning case, and toxic and fatal ... construct a calibration curve for DAEMS consisting of peak area ratio of DAEMS to IS on the vertical axis and DAEMS concentration on the horizontal axis A peak area ratio obtained from a test specimen...

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Drugs and Poisons in Humans - A Handbook of Practical Analysis (Part 20)

Ngày tải lên : 24/10/2013, 19:15

... 18 8 Cannabinoids and their metabolites GC analysis of cannabinoids in plant specimensa Reagents and their preparation • • • Extraction and purification of cannabinoids [3]: Cannabis sativa ... of ∆9-THC -11 -oic acid in urine at 50 ng/mL by immunoassay and the identifiable value of the acid by mass spectral measurements at 15 ng/mL Cases of analysis [13 ] Case 1: A 22-year-old male was ... ∆9-THC -11 -oic acid after the TMS and methyl ester-TMS derivatizations 19 1 19 2 Cannabinoids and their metabolites ⊡ Table 2 .1 Diagnostic ions in mass spectra of ∆9-THC -11 -ioc acid, 5α-cholestane and...

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Drugs and Poisons in Humans - A Handbook of Practical Analysis (Part 21)

Ngày tải lên : 24/10/2013, 19:15

... time of a peak of a specimen with that of the authentic standard and also by the confirmation of the absence of such a peak in a blank specimen An HPLC chromatogram for the authentic compounds ... commercially available (GL-SPE Vacuum Manifold, GL Sciences, Tokyo, Japan and some manufacturers in USA); it enables the attachment of 12 cartridges, and the simultaneous washing, elution and drying of the ... specimen obtained from a healthy subject and the urine specimens spiked with 0 .1 mL each of the standard solutions (2, and 20 µg/mL) are also handled in the same way as above ii Each of the above solution...

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Drugs and Poisons in Humans - A Handbook of Practical Analysis (Part 70)

Ngày tải lên : 24/10/2013, 19:15

... of a case J Forensic Sci 24:768–7 71 3) Tanaka J, Horigome H, Imai H et al (19 96) A case of severe methemoglobinemia for a newborn baby caused by well water Jpn J Pediatr 49 :16 61 16 65 (in Japanese) ... (19 71) Methemoglobinemia associated with well water JAMA 216 :16 42 16 43 11 ) Colomy HH (19 87) Cyanosis in infants caused by nitrates in well water JAMA 257:2788–2792 12 ) Fan AM, Steinberg VE (19 96) ... listlessness and metabolic acidosis coma, convulsive attack and hypotension death A poisoning case [4] An unidentified male was found naked from the waist up in a park at about 10 :00 p m.; he was suffering...

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Drugs and Poisons in Humans - A Handbook of Practical Analysis (Part 71 and End)

Ngày tải lên : 24/10/2013, 19:15

... 14 3, 15 3 headspace extraction 13 5, 14 3, 16 4, 16 7 headspace gas chromatography (HS-GC) 11 3 headspace GC/MS 437 headspace method 16 0, 438 headspace SPME 12 4, 12 7, 16 1, 16 4 headspace SPME-GC 12 6, 12 9 ... suaveolens 516 Datura ferox 516 Datura metel 509, 515 Datura stramonium 516 Datura tatula 516 DB -1 135, 14 4, 15 6, 16 0, 16 7, 19 0, 19 7, 2 31, 2 61, 303, 316 , 384, 537, 563, 593, 620, 650 DB-5 78, 17 4, ... 229, 4 91, 494, 495 calcium hypochlorite 403 calcium oxalate 452 camphor 443 cannabichromene 18 9 cannabidiol 18 7 cannabinoids 18 7 cannabinol 18 7 cannabis 18 7 Cannabis sativa L 18 7 Capcell Pak C18...

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Drugs and Poisons in Humans - A Handbook of Practical Analysis (Part 22)

Ngày tải lên : 29/10/2013, 01:15

... and BE after derivatization Setting up of cutoff values are very common in USA and Europe as a part of QC (quality control) and QA (quality assurance) system; the idea is useful to suppress the ... methods of administration, the relative amounts of unchanged cocaine, EME and BE excreted into urine are 1 14 %, 12 –60 % and 14 –55 % of total amount of cocaine administered, respectively [16 , 18 , 19 ] ... interval (period between death and autopsy) and the in vitro interval (period between sampling and analysis) are variable; the hydrolytic rate of cocaine shows great variation Usually, the metabolism,...

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Drugs and Poisons in Humans - A Handbook of Practical Analysis (Part 23)

Ngày tải lên : 29/10/2013, 02:15

... about A 10 -mL volume of ethanol and 10 mL distilled water are passed through a Sep-Pak C18 cartridge using a 10 -mL volume glass syringe to activate the cartridge at a flow rate not faster than ... concentration in the horizontal axis and peak area ratio of pentazocine to IS in the vertical axis The peak area ratio of a test specimen is applied to the calibration curve to obtain its pentazocine ... concentration Assessment of the method > Table 5 .1 shows EI mass spectra of pentazocine and IS The base peaks unfortunately appeared in a low mass range at m/z 70 and 59, respectively Therefore, the...

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Drugs and Poisons in Humans - A Handbook of Practical Analysis (Part 24)

Ngày tải lên : 08/11/2013, 01:15

... Tokyo, pp 10 8 10 9 (in Japanese) 2) The Pharmaceutical Society of Japan (ed) (19 92) Standard Methods of Chemical Analysis in Poisoning – With Commentary – Nanzando, Tokyo, p 43 and p 15 1 (in Japanese) ... method An EI mass spectrum of LSD is shown in > Fig 6 .1 The molecular ion appears as the base peak Fragment peaks can be observed at m/z 2 21, 207, 18 1 and 16 7 The fragmentation pathways are shown ... blood and urine, because its amount to be ingested is as small as about 10 µg and LSD is rapidly metabolized in human bodies As metabolites of LSD, 2-oxo-LSD, 3-, 13 - and 14 -hydroxy-LSDs and an...

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Drugs and Poisons in Humans - A Handbook of Practical Analysis (Part 25)

Ngày tải lên : 08/11/2013, 01:15

... MDMA 11 0, MA 1. 7, ketamine MDMA 13 0 MDMA 65 MDMA 98 MDMA 16 0 MDMA 93 MDMA 90 MDMA 13 0 MDMA 14 0 MDMA 52 MDMA 89, MA 1. 0, AP 6.9, ketamine, caffeine MDMA 60 MDMA 98 MDMA 28, MDEA 49 MDA 86 8 .1 8.2 ... Nishikawa M et al (19 91) Determination of methamphetamine and amphetamine in urine by headspace gas chromatography/mass spectrometry Anal Sci 7 :19 –22 25) Shima N, Kamata T, Nishikawa M et al Examination ... from the intestinal tract and reaches its peak concentration in plasma about h after oral administration [ 21, 22] The doses of 50, 75 and 12 5 mg in the usual “recreational” range for healthy human...

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Drugs and Poisons in Humans - A Handbook of Practical Analysis (Part 26)

Ngày tải lên : 08/11/2013, 01:15

... than The calibration curve is composed of PCP concentration on the horizontal axis and peak area ratio of PCP to IS on the vertical axis The peak area ratio of a test specimen is applied to the ... to a 15 -mL glass vial g vi The vial is capped with a Teflon-coated silicone rubber stopper and sealed with an aluminum cap vii The vial is heated at 10 0 °C for 15 on a heating block and mL of the ... Lee LF, Halzhauer LB et al (20 01) Analysis of urine samples in cases of alleged sexual assault: case history In: Salamore SJ (ed) Benzodiazepines and GHB: Detection and Pharmacology Humana Press,...

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