Drugs and Poisons in Humans - A Handbook of Practical Analysis (Part 67)

... toxicity of VX in humans; there are only estimated values based on the experimental GC/MS analysis for DAEMS in serum. (a) a total ion chromatogram (TIC) and a mass chromato-gram; (b) an EI mass ... secondary exposure for an analyst; the manipulations including the above evaporation should be done inside a dra chamber.f) For quantitative analysis of DAEMS, various concentrations of DAEMS are ... [18].GC/MS analysis for EMPA in serum. (a) a TIC and mass chromatograms; (b) an EI mass spectrum of the t-BDMS derivative of EMPA; (c) a CI mass spectrum of the same derivative of EMPA.⊡ Figure...

Drugs and Poisons in Humans - A Handbook of Practical Analysis (Part 17)

... they are also used as aromatics. Because of their pharmacological e ect, alkyl nitrites are being abused as uncontrolled inhalant drugs and causing a social problem [4]. Although there are many ... mg/mL), and kept airtightly in a refrigerator. A 5- L volume of the above solution is placed using a microsyringe in a glass vial containing 1 mL of dimethyl sulfoxide (DMSO), capped airtightly and ... specimen). In principle, the sampling, extraction and GC analysis should be made at low temperature, in a gastight state and in a short time.  is method is applicable to other biomedical specimens and...

Drugs and Poisons in Humans - A Handbook of Practical Analysis (Part 20)

... 2.3EI mass spectra of ∆9-THC, CBD, CBN and 5α-cholestane. GC analysis of cannabinoids in plant specimens190 Cannabinoids and their metabolites GC/MS analysis of ∆9-THC-11-oic acid in urine ... resin of the cannabis plant. Since the main component of cannabis, ∆9-tetrahydrocannabi-nol ( ∆9-THC), has various psychopharmacological e ects including hallucination, the can-nabis and ... their metabolites GC analysis of cannabinoids in plant specimens a Reagents and their preparation• Extraction and puri cation of cannabinoids [3]: Cannabis sativa L. is being grown at Hokuriku...

Drugs and Poisons in Humans - A Handbook of Practical Analysis (Part 21)

... concentrations206 Morphine and its analogues 8) Matsubara K, Fukushima S, Akane A et al. (1992) Increased urinary morphine, codeine and tetrahydropapavero-line in Parkinsonian patient undergoing L-3,4-dihydroxyphenylalanine ... pp 230–234 (in Japanese)196 Morphine and its analoguesMain metabolic pathways of morphine, heroin and codeine. The thick and thin arrows show the main and minor metabolic pathways, respectively.⊡ ... Nakajima K, Igarashi K et al. (1992) Analysis of morphine-3-glucuronide in urine by LC/APCI-MS. Eisei Kagaku 38:121–126 (in Japanese with an English abstract) 14) Tatsuno M, Nishikawa M, Katagi...

Drugs and Poisons in Humans - A Handbook of Practical Analysis (Part 70)

... methemoglobinemia be-comes severe, it causes cyanosis, headache, easy fatigability, respiratory and conciousness dis-turbances and  nally death.  e fatal methemoglobinemia is rare, but fatal ones a ... GC.vi. Various known amounts of nitrate and a  xed amount of IS are added to blank specimens and processed in the same way to construct a calibration curve.  e peak area ratio of nitrate to ... chapter, a method for GC analysis of nitrate and nitrite in blood using wide-bore and medium-bore capillary columns a er their derivatiza-tion with mesitylene b is presented.Reagents and...

Drugs and Poisons in Humans - A Handbook of Practical Analysis (Part 71 and End)

... neoovoidea 480Amanita pantherina 469Amanita phalloides 469Amanita verna 469, 474Amanita virosa 469, 473amanitin 473, 477, 479amido-type local anesthetic 3851-amino- 4- phenylbutane 1732-amino-6-hydroxymethyl-8-hydroxyquinazoline ... 327N-de-ethyl-LSD 228n-decane 165n-heptane 165n-hexane 165N-methyl- 1-( 3,4-methylene-dioxyphenyl )-2 -butan-amine 229N-methyl- 1-( 3,4-methylene-dioxyphenyl )-3 -butan-amine 233N-methyl-bis(tri uoro-acetamide) ... poisoning 104hydroxyl aprenolol 37314-hydroxy-LSD 2284-hydroxy-3-methoxy-amphetamine 2304-hydroxy-3-methoxy-ethylamphetamine 2384-hydroxy-3-methoxy-methamphetamine 2309-hydroxymethyl-1 0- ...

Drugs and Poisons in Humans - A Handbook of Practical Analysis (Part 22)

... of his ingestion and death. In addi-tion, the ratios of cocaine to BE in blood and in the brain, and the brain-to-blood ratios of cocaine and BE were compared with those described in literature ... mass spectra of the authentic cocaine, EME and BE a er derivatization.Setting up of cuto values are very common in USA and Europe as a part of QC ( quality control) and QA ( quality assurance) ... vitro interval (period between sampling and analysis) are variable; the hydrolytic rate of cocaine shows great variation. Usually, the metabolism, metabolite accumulation and excretion for cocaine...

Drugs and Poisons in Humans - A Handbook of Practical Analysis (Part 23)

... commercially avail-able.ii. Preparation • Pentazocine and dextromethorphan solutions: the drugs are separately dissolved in appro-priate amount of methanol; a 10–20 µL aliquot was added to 1 mL of ... the calibration curve, which is composed of pen-221tazocine concentration in the horizontal axis and peak area ratio of pentazocine to IS in the vertical axis.  e peak area ratio of a test ... pH to about 8.ii. A 10-mL volume of ethanol and 10 mL distilled water are passed through a Sep-Pak C18 cartridge using a 10-mL volume glass syringe to activate the cartridge at a  ow rate...

Drugs and Poisons in Humans - A Handbook of Practical Analysis (Part 24)

... digestive tract is rapid and distinct visual hallucination takes place 45 min–1 h a er oral intake of about 20 µg of LSD [1].  e hallucination becomes most marked 2–3 h a er the intake and lasts ... powerful hallucinogenic drugs of abuse. LSD was explosively abused in U.S .A. in the latter half of the 1960s. In Japan, the amount of seizure of LSD is much smaller than that of methamphetamine. ... under an o cial transfer process. • p-Dimethylbenzaldehyde reagent: a 0.125-g aliquot of p-dimethylaminobenzaldehyde (Wako Pure Chemical Industries, Ltd., Osaka, Japan and other manufacturers)...

Drugs and Poisons in Humans - A Handbook of Practical Analysis (Part 25)

... H, Nakajima K, Nishikawa M et al. (1991) Determination of methamphetamine and amphetamine in urine by headspace gas chromatography/mass spectrometry. Anal Sci 7:19–22 25) Shima N, Kamata T, ... hyperthermia, rhabdomyolysis, acute renal failure, dis-seminated intravascular coagulation and death [19, 20]. A detailed review by Kalant [16] re-vealed that 87 MDAs-related fatalities were associated ... Mental Health Services Administration (SAMHSA) is 250 ng/mL.Symptoms, and toxic and fatal concentrationsMDMA causes increased catecholamine (including serotonin) release and blockade of reuptake...

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