Introduction to Modern Liquid Chromatography, Third Edition part 1 pdf
Introduction to Modern Liquid Chromatography, Third Edition part 1 pdf
... ABBREVIATIONS xxxv 1 INTRODUCTION 1 1 .1 Background Information, 2 1. 1 .1 What Is HPLC?, 2 1. 1.2 What Can HPLC Do?, 4 1. 2 A Short History of HPLC, 6 1. 3 Some Alternatives to HPLC, 8 1. 3 .1 Gas Chromatography ... Special Forms of HPLC, 12 1. 4 Other Sources of HPLC Information, 12 1. 4 .1 Books, 12 1. 4.2 Journals, 13 1. 4.3 Reviews, 13 1. 4.4 Short Courses, 13 1. 4.5 The Internet, 13 References, 15 2 BASIC CONCEPTS ... Reciprocating-Piston Pumps, 10 43.5 .1. 1 Dual-Piston Pumps, 10 83.5 .1. 2 Accumulator-Piston Pumps, 10 83.5 .1. 3 Active Check Valve, 10 93.5.2 On-line Mixing, 10 93.5.2 .1 High-Pressure Mixing, 10 93.5.2.2...
- 10
- 629
- 0
Introduction to Modern Liquid Chromatography, Third Edition part 95 pdf
... see also Autosamplersaccuracy, 11 5filled-loop, 11 4, 11 7, 11 8laminar flow, 11 5operation, 11 4partial-loop, 11 5, 11 8Inlet-line frit, 90In-line filter, 10 3Inorganic particles, 214 – 217 Installation ... limitsdrift, 15 3–55electrochemical, 17 0 17 2error sources, 509flow cell, 15 0, 16 1fluorescence, 16 7 17 0quenching, 17 0FTIR, 19 1 19 2heat exchangers, 15 0hyphenated, 15 2, 18 5, 19 1light-scattering, 18 0 18 4evaporative ... 507LIMS, 12 8method-development software, 12 8 Part 11 compliant, 13 0report generation, 13 0sampling rate, 12 9, 15 4 15 5, 5 01 503signal measurement, 500– 516 system control, 12 9 21 CFR Part 11 , 13 0Daughter...
- 17
- 453
- 0
Introduction to Modern Liquid Chromatography, Third Edition part 4 pdf
... Leaks, 825 17 .4 .1. 4 Autosampler Leaks, 825 17 .4 .1. 5 Column Leaks, 828 17 .4 .1. 6 Detector Leaks, 828 17 .4.2 Abnormal Pressure, 830 17 .4.2 .1 Pressure Too High, 8 31 17.4.2.2 Pressure Too Low, 832 17 .4.2.3 ... CONTENTS 17 .3.5 Module Substitution, 820 17 .3.6 Put It Back, 8 21 17.4 Common Symptoms of HPLC Problems, 8 21 17.4 .1 Leaks, 822 17 .4 .1. 1 Pre-pump Leaks, 822 17 .4 .1. 2 Pump Leaks, 823 17 .4 .1. 3 High-Pressure ... 835 17 .4.3.5 Temperature Problems, 836 17 .4.3.6 Retention-ProblemSymptoms, 836 17 .4.4 Peak Area, 838 17 .4.4 .1 Peak Area Too Large, 839 17 .4.4.2 Peak Area Too Small, 840 17 .4.4.3 Peak Area Too...
- 10
- 488
- 1
Introduction to Modern Liquid Chromatography, Third Edition part 16 pdf
... today.3.5 .1. 2 Accumulator-Piston PumpsAn alternative design for the dual-piston pump is the accumulator-piston, ortandem-piston design shown in Figure 3 .13 d. In this case, one piston feeds intothe ... used to compensate for pump pulsations; today, the need for mechanical pulsedamping is due to low-pulse pump designs (e.g., dual-piston or accumulator-pistonpumps, Sections 3.5 .1. 1, 3.5 .1. 2). ... other piston at twice the flow rate. For example, if a flow rate of 1 mL/min wasdesired, the top piston (Fig. 3 .13 d) would pump at 1 mL/min. While the top pistondelivered solvent, the top (outlet)...
- 10
- 468
- 0
Introduction to Modern Liquid Chromatography, Third Edition part 17 pdf
... 20 15 0 4.6 5.0 10 ,000 90b (10 )c 18 0 (20) 1, 270 (13 0) 15 0 2 .1 5.0 10 ,000 20 (2) 40 (4) 265 (25) 10 0 4.6 3.0 11 ,10 0 60 (6) 11 5 (15 ) 800 (90) 10 0 2 .1 3.0 11 ,10 0 12 (2) 25 (15 ) 17 0 (20) 10 0 2 .1 1.8 ... 1. 8 18 ,500 9 (1) 20 (2) 13 0 (15 ) 10 0 1. 0 1. 8 18 ,500 2 (< ;1) 5 (< ;1) 30 (3)50 4.6 3.0 5,500 40 (4) 80 (10 ) 565 (60)50 2 .1 3.0 5,500 8 (1) 20 (2) 12 0 (80)50 1. 0 3.0 5,500 2 (< ;1) 5 (< ;1) ... (< ;1) 25 (3)50 4.6 1. 8 9,200 30 (4) 65 (7) 440 (50)50 2 .1 1.8 9,200 7 (1) 15 (2) 90 (10 )50 1. 0 1. 8 9,200 2 (< ;1) 3 (< ;1) 20 (2)aEquation (2.27), Vs/Vp0= 0 .16 ; note that the latter...
- 10
- 326
- 0
Introduction to Modern Liquid Chromatography, Third Edition part 19 pdf
... for leaks.REFERENCES 14 53. J. N. Brown, M. Hewins, J. H. M. van der Linden, and J. H. M Lynch, J. Chromatogr.,204 (19 81) 11 5.4. L. R. Snyder, J. Chromatogr. Sci., 21 (19 83) 65.5. J. Thompson, ... (2000) 17 49. 15 . R. G. Wolcott, J. W. Dolan, L. R. Snyder, S. R. Bakalyar, M. A. Arnold, and J. A.Nichols, J. Chromatogr. A, 869 (2000) 211 . 16 . J. W. Dolan, J. Chromatogr. A, 965 (2002) 19 5. 17 . ... Waeghe, J. Chromatogr. A, 756 (19 96) 21. 18 . Guidance for Industry: Part 11 , Electronic Signatures—Scope and Application,http://www.fda.gov/cder/guidance/index.htm (2003). 19 . J. J. Gilroy and...
- 10
- 442
- 0
Introduction to Modern Liquid Chromatography, Third Edition part 21 pdf
... CHARACTERISTICS 15 9Table4.2Typical Peak Volumes Vp0L (mm) dc(mm) dp(μm) Vp0(μL)a250 4.6 5 212 15 0 4.6 5 16 43 12 72 .1 3 26 10 0 4.6 3 10 42 .1 3 22 1. 0 3 52450 4.6 3 732 .1 3 15 2 .1 2 12 1. 0 ... limited value. 16 0 DETECTIONTable 4.4HPLC DetectorsSample-Specific(Sections 4.4–4 .10 )Bulk Property(Sections 4 .11 –4 .13 )Hyphenated(Sections 4 .14 –4 .15 )Reaction(Section 4 .16 )UV-visible ... plate height h = 2.5(seeEqs.2.27and3 .1) .Table 4.3UV-Detector Cell VolumesPath Length (mm) Inner Diameter (mm) Volume (μL) 10 1. 0 80.5 20.25 0.5 514 0.5 1 110 .80.5 0.2For best use over a wide...
- 10
- 271
- 0
Introduction to Modern Liquid Chromatography, Third Edition part 31 pdf
... CHROMATOGRAPHY FOR NEUTRAL SAMPLES(b)(a)log knn = n’ = 8iiiXXC 18 5 10 15 2025 1. 40 1. 38 1. 36αCH2n(c)(d )(e)(f ) 1. 30 1. 28 1. 26 1. 245 10 15 20 25nC8αCH2 1. 28 1. 24 1. 20C6 510 152025nαCH2C 1 1. 21 1 .17 1. 13 510 152025nαCH2Figure ... )(e)(f ) 1. 30 1. 28 1. 26 1. 245 10 15 20 25nC8αCH2 1. 28 1. 24 1. 20C6 510 152025nαCH2C 1 1. 21 1 .17 1. 13 510 152025nαCH2Figure 6.5 Retention as a function of alkyl chain length (for ... 257C 18 column40% ACN30°CC 18 column 60% ACN30°CC 18 column 40% ACN70°CCyano column40% ACN30°C(a)(b)(c)(d )C≡N (1) OCH3 (2)CH3 (3) 1 2332 1 1230 2 4 6 8 10 12 14 (min)0...
- 10
- 191
- 0
Introduction to Modern Liquid Chromatography, Third Edition part 52 pdf
... York, 19 98, pp. 218 –220.468 GRADIENT ELUTION02468 10 Time (min)20 15 10 25(a)(b)RPC0 -10 0% ACN/bufferHILIC3-40% buffer/ACN 12 NARP#26-29#7 -17 0246 810 Time (min) 10 5 1 1520 19 -29#7 -17 1- 6Figure ... Waeghe, J. Chromatogr. A, 756 (19 96) 21. 10 . P. Jandera and M.ˇSpaˇcek, J. Chromatogr., 366 (19 86) 10 7. 11 . L. R. Snyder and J. W. Dolan, J. Chromatogr. A, 799 (19 98) 21. 12 . A. P. Schellinger ... Section 17 .4.5 .1. CHAPTER TENCOMPUTER-ASSISTEDMETHOD DEVELOPMENT 10 .1 INTRODUCTION, 475 10 .1. 1 Basis and History of Computer Simulation, 478 10 .1. 2 When to Use Computer Simulation, 478 10 .2 COMPUTER-SIMULATION...
- 10
- 378
- 0
Introduction to Modern Liquid Chromatography, Third Edition part 65 pdf
... solvents (e.g 1 10 % methanol,propanol, or acetonitrile) can be added to the mobile phase to suppress hydrophobic 13 .4 SEPARATION OF PEPTIDES AND PROTEINS 599(a)(b)(c)20 10 02468 4 6 8 10 102pI ... exchanger more than (Fig. 13 .15 c).As a guideline, anion-exchange separations are often carried out at 1 to 1. 5 pHunits above a protein’s pI, and cation-exchange separations at 1 to 1. 5 pH unitsbelow ... relative to other modes of col-umn chromatography. Three other chromatographic techniques (chromatofocusing,hydroxyapaptite chromatography, and immobilized-metal affinity chromatography;Sections 13 .4.2.3 13 .4.2.5)...
- 10
- 361
- 0
Từ khóa: introduction to linear algebra third edition gilbert strang pdfintroduction to network simulator ns2 2nd edition downloadintroduction to network simulator ns2 2nd edition pdfintroduction to network simulator ns2 2nd editionintroduction to network simulator ns2 2nd edition free downloadintroduction to oracle9i pl sql part 1 pdfintroduction to visual basic 2008 express edition pdfintroduction to linear algebra strang 3rd editionprogramming in python 3 a complete introduction to the python language second editionintroduction to linear algebra strang 3rd edition solutionsintroduction to computer peter norton 7th edition pdfintroduction to java programming comprehensive 9th edition pdf free downloadship or sheep third edition part 5 docc how to program third edition türkçe deitel pdfintroduction to java programming comprehensive 9th edition solutionsNghiên cứu sự biến đổi một số cytokin ở bệnh nhân xơ cứng bì hệ thốngBáo cáo quy trình mua hàng CT CP Công Nghệ NPVNghiên cứu tổ hợp chất chỉ điểm sinh học vWF, VCAM 1, MCP 1, d dimer trong chẩn đoán và tiên lượng nhồi máu não cấpMột số giải pháp nâng cao chất lượng streaming thích ứng video trên nền giao thức HTTPNghiên cứu vật liệu biến hóa (metamaterials) hấp thụ sóng điện tử ở vùng tần số THzNghiên cứu tổ chức chạy tàu hàng cố định theo thời gian trên đường sắt việt namđề thi thử THPTQG 2019 toán THPT chuyên thái bình lần 2 có lời giảiGiáo án Sinh học 11 bài 13: Thực hành phát hiện diệp lục và carôtenôitGiáo án Sinh học 11 bài 13: Thực hành phát hiện diệp lục và carôtenôitGiáo án Sinh học 11 bài 13: Thực hành phát hiện diệp lục và carôtenôitĐỒ ÁN NGHIÊN CỨU CÔNG NGHỆ KẾT NỐI VÔ TUYẾN CỰ LY XA, CÔNG SUẤT THẤP LPWANNGHIÊN CỨU CÔNG NGHỆ KẾT NỐI VÔ TUYẾN CỰ LY XA, CÔNG SUẤT THẤP LPWAN SLIDEPhát hiện xâm nhập dựa trên thuật toán k meansNghiên cứu khả năng đo năng lượng điện bằng hệ thu thập dữ liệu 16 kênh DEWE 5000Thơ nôm tứ tuyệt trào phúng hồ xuân hươngTăng trưởng tín dụng hộ sản xuất nông nghiệp tại Ngân hàng Nông nghiệp và Phát triển nông thôn Việt Nam chi nhánh tỉnh Bắc Giang (Luận văn thạc sĩ)Chiến lược marketing tại ngân hàng Agribank chi nhánh Sài Gòn từ 2013-2015HIỆU QUẢ CỦA MÔ HÌNH XỬ LÝ BÙN HOẠT TÍNH BẰNG KIỀMMÔN TRUYỀN THÔNG MARKETING TÍCH HỢPQUẢN LÝ VÀ TÁI CHẾ NHỰA Ở HOA KỲ