... Purge- and- Trap and Extraction for Volatile Organics in Soil and Waste Samples,” and Method 5021, Volatile Organic Compounds in Soils and Other Solid Matrices Using Equilibrium Headspace Analysis,” ... be included in a quality assurance project plan (QAPP) or sampling and analysis plan (SAP). 2.0 PURPOSE EPA Region 9 has developed technical guidelines to help ensure that sampling and analyzing ... for Testing and Materials (2003) Standard Guide for Sampling Waste and Soils for Volatile Organic Compounds, ASTM Guide D 4547-03 Grant, C.L., T.F. Jenkins, and A. R. Mudambi (1996) Comparison...